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Laboratory Tips Safety proceedures, test reagents, drilling rubber stoppers, bending glass tubes, etc. Contributed to by chemists.

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 #1 
Old 2002-12-11, 10:42
kraka kraka is offline
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Default cloral hydrate

can some one give me a link or post the recipie for cloral hydrate, please do not post a link to rhodium and please please do not flame me as this board has a notorious reputation for it. ps anyone know where to get calcium oxide. any reply will be grounds for a life long commitment to this board and its posters in helping out anyway i can.
oh and if u know can anyone give me a link to a good mescaline extract if one exists, i have tried many hours to find a good one yet remain unsuccessful
 #2 
Old 2002-12-11, 16:10
the creator the creator is offline
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Default Re: cloral hydrate

Rhodium is about the only place I have ever seen a chloral hydrate synth (but then again I have never really searched). Is there something you dont understand about the synth on rhodium?
 #3 
Old 2002-12-11, 18:06
tryptamine tryptamine is offline
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Default Re: cloral hydrate

Yeah that is the only synth that I have ever heard of too, why would you want this anyways? It sounds like you are a serious newbie chemist but this is a ridiculous thing to want to make, unless it is just for the experience.

Calcium oxide can be bought from the pharmacy, it is a pretty common chemical in industry though and is used in huge amounts.
 #4 
Old 2002-12-14, 08:49
kraka kraka is offline
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Default Re: cloral hydrate

thanks for the replies, the synth on that site is pretty easy and i understand it fully except for the bit where u produce the chlorine gas. it sez 2" of chlorine bleach to i tablespoon of ammonia or somethin. what the hell is 2" ? im not sure whether it has something to do with the imperial system or whatever coz i only know metric measurements...
 #5 
Old 2002-12-14, 08:51
kraka kraka is offline
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Default Re: cloral hydrate

oh yeah and its totally jsut for the experience, a friend of mine sez i need to learn to be able to safely control chemical reactions before i move onto bigger and better things, is this good advice or just bull shit?
 #6 
Old 2002-12-14, 17:23
tryptamine tryptamine is offline
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Default Re: cloral hydrate

Well you should get experience in all the chemistry you can before you work on something important, your friend gives good advice.

I just about killed myself with a chlorine generator once, they aren't super dangerous, I was just being stupid, so do it outside and it really doesn't matter what amounts of bleach and Hydrochloric acid you use(molar ratio 1:1 would be good) just be aware that it is a very vigorous reaction and you might want to control the addition of acid.

good luck,
bee safe.
 
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