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Laboratory Tips Safety proceedures, test reagents, drilling rubber stoppers, bending glass tubes, etc. Contributed to by chemists.

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 #1 
Old 2001-07-06, 00:32
acidmelt acidmelt is offline
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Default Slp-- Gooey chilli needs help.

SLp-- Up till like 2 dreams ago everything was going perfect, perfect ph, perfect pre-cursers, everything. Anyhow on my last few dreams (basic p/p Hi reduction) Everything seems to go fine until crystalization, then it kinda of stays gooey and doesnt crystalize well. My ph papers in my dream said that it was the right ph (around 6.5 to 7.4) so why is it not crystalizing correctly? Would this be from precurser impurities, or from something else? I am sure that i cooked it long enough in my dream (1hr 40min). it was at a range of 150F to 180F at the peak. I have dreamed this same dream a whole hell of a lot of times in the past and it always has came out perfect, but not these last 2 times. Any ideas what is happening?
 #2 
Old 2001-07-06, 01:59
madmatt madmatt is offline
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Default Re: Slp-- Gooey chilli needs help.

If the stuff in your dream is brown the reaction went long enough to accomplish the change but you still have unreacted I in the mix. Don't know what you can do about it but I do know thiosulfate is just sweeping the dirt under the carpet and is a waste of time. If the stuff is clear you didn't spend enough time on your pills.
 #3 
Old 2001-07-06, 02:29
acidmelt acidmelt is offline
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Default Re: Slp-- Gooey chilli needs help.

no theres no excess I2 left. its perfectly clear. I did a pretty basic extract for the E it seemed really clean. I had gotten out all binders in my dream and it looked to be of a decent purity. In this dream I did use cheap ass pills. but i had never had problems with using these certain pills in the past.
 #4 
Old 2001-07-06, 13:21
nihilistic nihilistic is offline
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Default Re: Slp-- Gooey chilli needs help.

well how did it look before the a/b? maybe you needed to place on a light boil for a while, as it sounds like some tell tale signs of unreacted E.

i dont know, have you a/b the goey stuff again? i find that might help.

or do a worlok recystilization, dissolve in alcho untill the first sign of a skin etc, then add fresh alcho, and 20 ml of acetone, and place in frezzer over night.

that will turn your goey chili into crystals,
it worked with our strange looking stuff, similar to that.???

???????????
 #5 
Old 2001-07-07, 04:09
acidmelt acidmelt is offline
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Default Re: Slp-- Gooey chilli needs help.

you got the wrong idea here. i know how to fix it, I was just looking for ideas on what was wrong with these last 2 dreams. It was cooked for quite a long time and there was no unreacted E. It turned out to be REALLY pure crystal after I fixed it so thats why i know it was all reacted. Everything was done perfect, in my mind anyhow. i have done it this exact way (in my dreams) multiple times and it has always turned out PERFECT. I mean it was done with persicion and care exactly the same every time. I just dont get it. it just boogles my fuckin mind. (and pisses me off too) so anyhow please give up some ideas and thanks for everyones input. for now on i am going to dream about getting my Hi going ahead of time and bust out some nice long refluxes. but i am just looking for ideas.... thanks for your input.

nih. - it was crystal clean and clear after the a/b of course. i would never settle for anything less! :-) by the way what is the strange looking stuff that you are talking about?
 #6 
Old 2001-07-09, 00:45
brad777 brad777 is offline
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Default Re: Slp-- Gooey chilli needs help.

the magic no is 7.1..stablize...dh20..also..1 hr 40minutes will work only if amount is say under 70g..2hr 15minutes is a better dream ..non stik frypan...acetone...etc.1 dream per night only..not 2 dreams..start to finito..bad pills..how much fat during cool down..more than last dream???..no such thing as bad pills just bad filtering,put 1st 20% of receiver back in mix??try splash head
 #7 
Old 2001-07-09, 00:49
brad777 brad777 is offline
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Default Re: Slp-- Gooey chilli needs help.

150-180..get outta town..stop being a big bubble boy...throw temp rod away..light simmer boil..135 would be better and only from 1st bubble do we time
 #8 
Old 2001-07-10, 11:54
slpwlkr333 slpwlkr333 is offline
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Default Re: Slp-- Gooey chilli needs help.

in this dream.... can you recall what was holding the pfed together; the binders, or just the pill name. im looking for a nice clean allergy and energy pill and ill go with instinct i guess cause im at ends.
 #9 
Old 2001-07-11, 16:42
acidmelt acidmelt is offline
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Default Re: Slp-- Gooey chilli needs help.

all right i will try to keep it going for longer at 135 instead of 150-180 in my next dream. thanks for the tips.

i didnt keep any of the boxes in my dream so I dont remember the binders. there was no providone though, i do remember that.
 
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