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| Laboratory Tips Safety proceedures, test reagents, drilling rubber stoppers, bending glass tubes, etc. Contributed to by chemists. |
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# 1

2008-09-25, 03:54
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green powder after electrolysis
I'm using a steel nail and some NaCl for my electrolysis and it's creating a green or black powdery substance at the bottom of the container. At the top of course is the iron oxide. Does anyone know what this powder is?
Edit:Also would using about a tablespoon of salt create enough chlorine gas that I should stop it?
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# 2

2008-09-25, 06:43
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Regular
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Beneath a scanner, darkly.
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Re: green powder after electrolysis
Do the equation, and the answers shall become apparent.
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# 3

2008-09-25, 14:04
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Re: green powder after electrolysis
The thing is I don't know the exact composition in the nail. All I know is that there is iron in it.
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# 4

2008-09-25, 14:17
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Regular
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the happy land of australia
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Re: green powder after electrolysis
you have a nail in salt water, and your running a current through it?
why?
yeah, i assume your just rusting the nail, and the stuff collecting is one of the many possible iron oxides.
if you want a proper answer you will have to do the chemistry or at least explain exactly what you were doing.
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# 5

2008-09-25, 21:24
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Regular
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mah compound
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Re: green powder after electrolysis
Possibly a copper salt?
__________________
http://beesafe.goshopper.net/ For all your test reagent needs! Bee Safe!
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# 6

2008-09-25, 22:02
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Re: green powder after electrolysis
nope no copper in the nail. Probably just wet iron oxide I guess..
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# 7

2008-09-26, 08:41
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Re: green powder after electrolysis
I submit: Ferrous chloride tetrahydrate
just guessing mind...
http://www.languangchem.com/pages/product-e1.htm
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# 8

2008-09-28, 11:34
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Regular
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Beneath a scanner, darkly.
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Re: green powder after electrolysis
Quote:
Originally Posted by Captain Generic
nope no copper in the nail. Probably just wet iron oxide I guess..
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No copper in the nail, but what kind of wire is running current through the nail? hmm?
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# 9

2008-09-28, 11:38
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Re: green powder after electrolysis
Electrolysis for what?
If you want electrodes that don't shed all the time, try clean carbon electrodes such as in carbon-zinc batteries in the center, and keep the connections out of the water ..
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# 10

2008-09-28, 11:50
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Regular
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the happy land of australia
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Re: green powder after electrolysis
The easiest place to get intert electrodes in by skinning a pencil. ive used them a few times when its been too diffcult to get anything better.
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#11
 2008-09-28, 19:09
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Re: green powder after electrolysis
Quote:
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Originally Posted by RAOVQ
The easiest place to get intert electrodes in by skinning a pencil. ive used them a few times when its been too diffcult to get anything better.
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That is graphite.
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#12
 2008-10-01, 07:44
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Regular
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Utah: Mountains, Mormons, Meth
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Re: green powder after electrolysis
A nickel salt? Nickel 3 is black and nickel 2 is green.
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#13
 2008-10-05, 23:33
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Some Old Drunk Guy 
Regular
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Re: green powder after electrolysis
Quote:
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Originally Posted by nshanin
A nickel salt? Nickel 3 is black and nickel 2 is green.
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This man is correct
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#14
 2008-10-06, 00:48
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Re: green powder after electrolysis
it's probably a mixture of iron oxides and iron chloride hydrates. Is the nail your cathode or the anode?
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