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Laboratory Tips Safety proceedures, test reagents, drilling rubber stoppers, bending glass tubes, etc. Contributed to by chemists.

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  #1   Add Captain Generic to your ignore list  
Old 2008-09-25, 03:54
Captain Generic Captain Generic is offline
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Default green powder after electrolysis

I'm using a steel nail and some NaCl for my electrolysis and it's creating a green or black powdery substance at the bottom of the container. At the top of course is the iron oxide. Does anyone know what this powder is?

Edit:Also would using about a tablespoon of salt create enough chlorine gas that I should stop it?
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  #2   Add FullMetalJacket to your ignore list  
Old 2008-09-25, 06:43
FullMetalJacket FullMetalJacket is offline
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Default Re: green powder after electrolysis

Do the equation, and the answers shall become apparent.
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  #3   Add Captain Generic to your ignore list  
Old 2008-09-25, 14:04
Captain Generic Captain Generic is offline
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Default Re: green powder after electrolysis

The thing is I don't know the exact composition in the nail. All I know is that there is iron in it.
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  #4   Add RAOVQ to your ignore list  
Old 2008-09-25, 14:17
RAOVQ RAOVQ is offline
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the happy land of australia
Default Re: green powder after electrolysis

you have a nail in salt water, and your running a current through it?

why?

yeah, i assume your just rusting the nail, and the stuff collecting is one of the many possible iron oxides.

if you want a proper answer you will have to do the chemistry or at least explain exactly what you were doing.
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  #5   Add stupid noob to your ignore list  
Old 2008-09-25, 21:24
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Default Re: green powder after electrolysis

Possibly a copper salt?
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http://beesafe.goshopper.net/ For all your test reagent needs! Bee Safe!
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  #6   Add Captain Generic to your ignore list  
Old 2008-09-25, 22:02
Captain Generic Captain Generic is offline
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Default Re: green powder after electrolysis

nope no copper in the nail. Probably just wet iron oxide I guess..
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  #7   Add fcknut to your ignore list  
Old 2008-09-26, 08:41
fcknut fcknut is online now
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Default Re: green powder after electrolysis

I submit: Ferrous chloride tetrahydrate

just guessing mind...

http://www.languangchem.com/pages/product-e1.htm
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  #8   Add FullMetalJacket to your ignore list  
Old 2008-09-28, 11:34
FullMetalJacket FullMetalJacket is offline
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Beneath a scanner, darkly.
Default Re: green powder after electrolysis

Quote:
Originally Posted by Captain Generic View Post
nope no copper in the nail. Probably just wet iron oxide I guess..
No copper in the nail, but what kind of wire is running current through the nail? hmm?
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  #9   Add scovegner to your ignore list  
Old 2008-09-28, 11:38
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Default Re: green powder after electrolysis

Electrolysis for what?

If you want electrodes that don't shed all the time, try clean carbon electrodes such as in carbon-zinc batteries in the center, and keep the connections out of the water ..
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  #10   Add RAOVQ to your ignore list  
Old 2008-09-28, 11:50
RAOVQ RAOVQ is offline
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the happy land of australia
Default Re: green powder after electrolysis

The easiest place to get intert electrodes in by skinning a pencil. ive used them a few times when its been too diffcult to get anything better.
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 #11 
Old 2008-09-28, 19:09
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mah compound
Default Re: green powder after electrolysis

Quote:
Originally Posted by RAOVQ
The easiest place to get intert electrodes in by skinning a pencil. ive used them a few times when its been too diffcult to get anything better.

That is graphite.
 #12 
Old 2008-10-01, 07:44
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Utah: Mountains, Mormons, Meth
Default Re: green powder after electrolysis

A nickel salt? Nickel 3 is black and nickel 2 is green.
 #13 
Old 2008-10-05, 23:33
Some Old Drunk Guy Some Old Drunk Guy is offline
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Default Re: green powder after electrolysis

Quote:
Originally Posted by nshanin
A nickel salt? Nickel 3 is black and nickel 2 is green.


This man is correct
 #14 
Old 2008-10-06, 00:48
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Default Re: green powder after electrolysis

it's probably a mixture of iron oxides and iron chloride hydrates. Is the nail your cathode or the anode?
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