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| Laboratory Tips Safety proceedures, test reagents, drilling rubber stoppers, bending glass tubes, etc. Contributed to by chemists. |
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# 1

2008-07-30, 07:58
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Regular
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Melbourne Australia
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Mescaline extraction.. Failed?
When defatting the fat layer was at the bottom instead of in the middle. Why?
And at the end when dripping water into the xylene to get the alkaloids into the water, the water dripped down to the bottom instead of staying at the top??
The finished product was yellowish crystals..
Was this a fail ?
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# 2

2008-07-30, 08:59
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Re: Mescaline extraction.. Failed?
Quote:
Originally Posted by Wog
When defatting the fat layer was at the bottom instead of in the middle. Why?
And at the end when dripping water into the xylene to get the alkaloids into the water, the water dripped down to the bottom instead of staying at the top??
The finished product was yellowish crystals..
Was this a fail ?
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You sound like a fail to me...
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# 3

2008-07-30, 09:05
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Regular
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Melbourne Australia
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Re: Mescaline extraction.. Failed?
You sound like you love cock?
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# 4

2008-07-30, 09:12
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Re: Mescaline extraction.. Failed?
Quote:
Originally Posted by Wog
You sound like you love cock?
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haha  actually sorry to disappoint you  Spunnn might like it tho'. Anyways, its funny because unlike you I:
a) Don't like cock
b) Can do a fucking A/B without fucking up
c) Can do research
Have a nice day and enjoy your mescaline...oh wait...bahahahha
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# 5

2008-07-30, 09:31
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Regular
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mah compound
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Re: Mescaline extraction.. Failed?
Cmon now, it's a legit question, and he did show due diligence. I even told him to come here with it myself. Just trying to drum up some conversation. Like BT was saying, this place used to be a lot of reaction or clean up questions, which I always loved, because it's how I learned quite a bit. I think with that, and the more advanced stuff we have going now, LT will be an excellent place for people of all stages of learning.
I just want to keep out the riff raff assholes who are so stupid you almost think they are trolling. Say whatever you want to those fuckers, but try to refrain from nailing the noobs with good intentions.
I want people to learn. So long as they show they are smart enough to do things safely, which this fellow has.
__________________
http://beesafe.goshopper.net/ For all your test reagent needs! Bee Safe!
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# 6

2008-07-30, 09:50
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Regular
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England
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Re: Mescaline extraction.. Failed?
I lol'd at the customary SoH response.
So you got crystals out of the AB?
Yellowy ones at that?
Have you even recrystallised once?
What do they dissolve in?
Are there enough to attempt a melting point test?
Could you scrounge together enough to run a ghetto TLC plate? (read: yes, search JPs threads)
I would say, first recrystallise, see what they look like, dunno if its the same as DMT, but an ice cold ammonia wash does wonders if they're still looking a little grimy. Then try to work out what they might be. I imagine a bit of test reagents may help you here, I seem to recall there was a response for mescaline.
Oh, and as a final tip that might be handy, read a certain thread on WD by Tramp, MEK should be easy enough to find. I think, I can't quite remember who did it, but it was a damn good thread, and gave excellent results.
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# 7

2008-07-30, 09:59
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Regular
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Melbourne Australia
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Re: Mescaline extraction.. Failed?
Whats WD?
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# 8

2008-07-30, 10:12
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Regular
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England
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Re: Mescaline extraction.. Failed?
Quote:
Originally Posted by Wog
Whats WD?
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http://www.totse.com/community/showthread.php?t=2063187
If you don't know what WDs is, its the most obvious acronym in that thread, and is linked to, and you'll need to create an account.
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# 9

2008-07-30, 10:20
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Regular
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mah compound
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Re: Mescaline extraction.. Failed?
Quote:
Originally Posted by Von Bass
http://www.totse.com/community/showthread.php?t=2063187
If you don't know what WDs is, its the most obvious acronym in that thread, and is linked to, and you'll need to create an account.
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Excellent, thank you for showing him that. Perfect.
__________________
http://beesafe.goshopper.net/ For all your test reagent needs! Bee Safe!
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# 10

2008-07-30, 10:39
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Regular
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Melbourne Australia
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Re: Mescaline extraction.. Failed?
lol, stupid noob you seem to be happy with me for some reason?
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#11
 2008-07-30, 10:51
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Re: Mescaline extraction.. Failed?
Quote:
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Originally Posted by Wog
lol, stupid noob you seem to be happy with me for some reason?
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Not you in particular, your thread. I saw it in BLTC and just had to snatch it up. It doesn't belong there, and you will get nothing but flames. It belongs HERE, and here is where you will get the best help. This forum is slow as fuck, and I know for a fact several of you get bored as hell, and have nothing better to do than research something, so that's why I brought it here. Er, had you bring it here, you know.
I've never looked into it, to be honest, I want to save my mescaline virginity for true peyote buttons.
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#12
 2008-07-30, 11:00
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stateofhack 
Regular
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Re: Mescaline extraction.. Failed?
Excellent, thank you for showing him that. Perfect.
Someone is happy, have you been making hydrocodone following the nice method Von Bass posted ;)
lol
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#13
 2008-07-30, 11:10
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Re: Mescaline extraction.. Failed?
Someone is happy, have you been making hydrocodone following the nice method Von Bass posted ;)
lol
LOL no need to waste my time with that, I get a gram of it every month from my doctor for about five bucks.
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#14
 2008-07-30, 11:10
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Wog 
Regular
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Re: Mescaline extraction.. Failed?
Im thinkin' i just fucked up the PH levels.. Every PH tester i could find wouldnt show under 6.2 or over 10..
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#15
 2008-07-30, 11:19
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Re: Mescaline extraction.. Failed?
Quote:
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Originally Posted by Wog
Im thinkin' i just fucked up the PH levels.. Every PH tester i could find wouldnt show under 6.2 or over 10..
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http://search.ebay.com/search/search.dll?sofocus=bs&sbrftog=1&dfsp=3&catref=C12&satitle=ph&sacat=26413%26catref%3DC6&sadis=200&fpos=40215&sabfmts=1&ftrt=1&ftrv=1&saprclo=&saprchi=&seller=1&sass=viperctw&fsop=3%26fsoo%3D1&coaction=compare&copagenum=1&coentrypage=search
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#16
 2008-07-30, 11:33
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stateofhack 
Regular
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Re: Mescaline extraction.. Failed?
LOL no need to waste my time with that, I get a gram of it every month from my doctor for about five bucks.
Bastard!
Im thinkin' i just fucked up the PH levels.. Every PH tester i could find wouldnt show under 6.2 or over 10..
Ok, lets try this again, i will try to be nice :) add me on msn if you want some help (stateofhack@hotmail.com). Did you calibrate your PH meter before using it? I had that happened to me once :(
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