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Better Living Through Chemistry Discussions of any and all sorts of mind-warping chemicals, pills, booze, mind machines, trippy stuff, current street prices, importing pharmaceuticals, smart drugs, nutrients, herbs, and altered states. Please try to keep your conversations "theoretical" in nature, since this is an open conference.

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 #1 
Old 2008-04-02, 23:42
NEPHROSIS NEPHROSIS is offline
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Default evaporating 2ce solution?

I got some 2ce in a solution of water but I'm not sure how stable 2ce is...I want to reduce the volume, is it ok to just heat it straight without ruining it or how should I do it?
 #2 
Old 2008-04-03, 04:44
NEPHROSIS NEPHROSIS is offline
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Default Re: evaporating 2ce solution?

anyone??
 #3 
Old 2008-04-03, 05:16
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mah compound
Default Re: evaporating 2ce solution?

Gently heat it. Just put it in a shallow dish and set it on top of a TV or monitor or DVD player, and the heat coming off that will evaporate it. Using an oven you risk decomp if you go too high. I don't know HOW high you have to go, but the method I described is the safest quickest way to do it without losing product.


The key is having as large a dish as possible with as little lip on it as possible.


I would avoid direct heat if I were you, just to be safe.
 #4 
Old 2008-04-03, 05:29
NEPHROSIS NEPHROSIS is offline
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Default Re: evaporating 2ce solution?

Alright thanks.
 #5 
Old 2008-04-03, 05:30
Moderator
 
mah compound
Default Re: evaporating 2ce solution?

No prob.
 #6 
Old 2008-04-03, 06:59
Regular
 
Default Re: evaporating 2ce solution?

check melting/decomp point on phikal and set oven lower?
dunno if this would work...

to "bee safe" do the other method.
 #7 
Old 2008-04-03, 16:14
Moderator
 
mah compound
Default Re: evaporating 2ce solution?

Quote:
Originally Posted by bad_b0y_4_lif3
check melting/decomp point on phikal and set oven lower?
dunno if this would work...

to "bee safe" do the other method.



I don't recall PIHKAL having that info. An MSDS would though.
 #8 
Old 2008-04-03, 20:37
cr0w cr0w is offline
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Default Re: evaporating 2ce solution?

Preheat oven to "warm" or whatever the lowest is

Turn off oven

Stick in pyrex baking dish of solution
 
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