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| Laboratory Tips Safety proceedures, test reagents, drilling rubber stoppers, bending glass tubes, etc. Contributed to by chemists. |
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# 1

2007-05-30, 17:44
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Yes, I'm a chem n00b.
Sorry for the stupid question, but I basically have no chemistry knowledge. I know, I know "Read before you start" and I have. The problem is, I can only learn enough to fuck something up by reading. I'm a hands-on type of person.
That being said, is there anything I may find in my house that I could substitute for NaOH in a DMT extraction? I'll be doing a standard a/b, using distilled vinegar for my acid (I know, HCl is better, but I'm poor.) I'll buy the lye if I NaOH if I have to, but if there would be something common that could be substituted, I'd love to hear about it.
*Puts on flame-retardant suit*
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# 2

2007-05-30, 18:47
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Re: Yes, I'm a chem n00b.
Ammonia
edit- You might just be better of buying lye though, I don't think ammonia is too strong of a base.
Last edited by NEPHROSIS : 2007-05-30 at 18:48.
Reason: .
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# 3

2007-05-30, 20:19
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Re: Yes, I'm a chem n00b.
Yeah, I don't have any ammonia. Any other ideas? If I have to buy something, I'm just gonna get the lye.
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# 4

2007-05-30, 20:28
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Regular
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Re: Yes, I'm a chem n00b.
You can make your own lie with bacon fat  but you can research it you lazy bitch...or just buy NaOH: cheap easy to get and good for dmt extraction's 
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# 5

2007-05-30, 21:47
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Re: Yes, I'm a chem n00b.
Just get the NaOH. And HCl is much better, and if you have distilled acetic acid, you are damn sure wasting it if you use it on this.
What you SHOULD do, is take that acetic, add it to sodium bicarbonate, evaporate, and then distill it with sulfuric acid to yield damn near anhydrous acetic acid. THEN one could use that to acetylate morphine.
It's really easy as fuck, and a still kit is a MUST, so if you have one, and like opiates, and have access to morphine, go with that. I would be more than happy to help you out over msn or email if you like.
But again, go with the NaOH.
And I didn't flame you because I like your posts, from what I can remember, AND you've done your own research for the most part, and are coming here with a legitimate question.
Now if all the rest of you little bastards could follow suit.
See, I'm not a bad guy, I just hate lazy asses.
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# 6

2007-05-31, 00:08
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Regular
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USA
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Re: Yes, I'm a chem n00b.
How about gassing GAA with SO2 or SO3 to yield AA and sulfuric/ous acid?
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# 7

2007-05-31, 02:40
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Re: Yes, I'm a chem n00b.
Quote:
Originally Posted by stupid noob
Just get the NaOH. And HCl is much better, and if you have distilled acetic acid, you are damn sure wasting it if you use it on this.
What you SHOULD do, is take that acetic, add it to sodium bicarbonate, evaporate, and then distill it with sulfuric acid to yield damn near anhydrous acetic acid. THEN one could use that to acetylate morphine.
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So I really shouldn't bother with the vinegar? i'm just kind of doing a trial run here to get some experience, so I don't want to have to put out more money than I have to.
And thanks, but I'm good on the heroin. I just want some DMT for now.
Quote:
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I would be more than happy to help you out over msn or email if you like.
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I might take you up on that when the time comes.
Quote:
And I didn't flame you because I like your posts, from what I can remember, AND you've done your own research for the most part, and are coming here with a legitimate question.
Now if all the rest of you little bastards could follow suit.
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Thanks. I appreciate that.
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# 8

2007-05-31, 06:32
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Re: Yes, I'm a chem n00b.
Feel free to add me anytime. And I'm sure vinegar would work, but if you have distilled it, it would seem like a waste of precursors.
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# 9

2007-05-31, 06:41
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Re: Yes, I'm a chem n00b.
Quote:
Originally Posted by 36fuckin5
Yes, I'm a chem n00b.
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Eh, least you admit it. Not that it'll save you from being flamed if you're an idiot, but it's good for a small margin of leeway. Let's see how ya did...
Quote:
Originally Posted by 36fuckin5
Sorry for the stupid question, but I basically have no chemistry knowledge. I know, I know "Read before you start" and I have. The problem is, I can only learn enough to fuck something up by reading. I'm a hands-on type of person.
That being said, is there anything I may find in my house that I could substitute for NaOH in a DMT extraction? I'll be doing a standard a/b, using distilled vinegar for my acid (I know, HCl is better, but I'm poor.) I'll buy the lye if I NaOH if I have to, but if there would be something common that could be substituted, I'd love to hear about it.
*Puts on flame-retardant suit*
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Congratulations; you're better than most of the idiots I deal with. Thank you.
Incidentally, by reading your post, I presume you read recipies for a/b, rather than information on a/b. In short, any base strong enough to grab the acid will work.
Ammonia and baking soda come to mind. Not baking powder, which is usually a mix of crap, but sodium bicarbonate USB.
...or - since you mention poverty - you could make your own crude NaOH through aqueous extraction from wood ash, or something.
I, umm... presume your distilled vinegar is about 5%, and comes from the store, or did you distill it yourself?
...anyways... welcome to LT.
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# 10

2007-05-31, 06:46
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Re: Yes, I'm a chem n00b.
Quote:
Originally Posted by stupid noob
What you SHOULD do, is take that acetic, add it to sodium bicarbonate, evaporate, and then distill it with sulfuric acid to yield damn near anhydrous acetic acid. THEN one could use that to acetylate morphine.
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...y'know, I was always wondering, years ago, why people preferred acetic anhydride acetylation over sulfuric-acid catalyzed carboxolyc alkylation using morphine (or salycylic acid) as the alcohol in question...
Hmm. So, my musings were tested independently by others and worked like they logically should? Interesting... any links to lit on the yields?
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This thread continued for 3 pages in the real archive, 27 posts total - only page 1 survived here.
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