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Laboratory Tips Safety proceedures, test reagents, drilling rubber stoppers, bending glass tubes, etc. Contributed to by chemists.

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  #1   Add goodroad to your ignore list  
Old 2007-04-19, 09:50
goodroad goodroad is offline
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Talking got someones left overs

swim's friends got some left over but it has been sitting around for quite a while. Swims rriend tried to gas it but nothing came out, no snow at all. but swims friends friend swears that there is at least a quarter once left over..... its been sitting there for like 4 or five months will or is it still alright..? I know that the shit is still in there just looking foir the easiest way to get it out , can some one help this poor soul? its in good old coleman and when swigd's friend gased it dry as all hell no snow falling at all in the mix. aome one kick me down some info please.... Again help would be great you peeps at totse are the shit but you all know that of course.. Thanks again

Last edited by goodroad : 2007-04-19 at 09:55. Reason: for got to put some minor details in
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  #2   Add SpeedyDreamer to your ignore list  
Old 2007-04-19, 13:47
SpeedyDreamer SpeedyDreamer is offline
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Default Re: got someones left overs

Add about 200ml of TCE throw the lye to her shake well, let sit for about 30 min, pull TCE off the bottom (it will be the heaviest), run through filters till clear, gas away. Thats what Speedy would try. If that doesn't work, there may not be anything there. TCE is a lot stronger puller than colemans plus it's easier to migrate down than it is up.
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  #3   Add UK_TOM to your ignore list  
Old 2007-04-19, 13:47
UK_TOM UK_TOM is offline
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Default Re: got someones left overs

Was it sitting on top of the based fluid for months or was it based and and the NP removed with the freebase in it???
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  #4   Add goodroad to your ignore list  
Old 2007-04-20, 03:17
goodroad goodroad is offline
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Talking Re: got someones left overs

Quote:
Originally Posted by UK_TOM View Post
Was it sitting on top of the based fluid for months or was it based and and the NP removed with the freebase in it???
right now there are two layers swigds friend put dh20 in to the NP so thee are to layers with snot floating around. this was gased once be for to get the free base but before hand was sitting in NP for months.
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  #5   Add gigster to your ignore list  
Old 2007-04-20, 06:50
gigster gigster is offline
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Default Re: got someones left overs

So another day what do you wanna do bill? Ah fuck who knows bob, lets go over to jimmys and see whats going on.
Alright lets go.

And so bill, bob , and jimmy are hanging when jimmy says: "hey you guyz want some NP solvent?" "its been sitting around here for a while,its got at least 1\4 oz in it,just need to gas it out". " I would but its only worth about $700.00 so I dont want it"

Bill checks with bob "ya wanna take it" bob replies "yeah ok

Hey jimmy a couple of your plants look like they only have about a 1\2lb of bud " "can we have those too?"

jimmy says oh yeah go ahead

Who the fuck would gas out part and not all of it then give it away? someones laughing their ass off
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  #6   Add UK_TOM to your ignore list  
Old 2007-04-20, 08:46
UK_TOM UK_TOM is offline
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Default Re: got someones left overs

Yeah, true Gigster - it wouldn't make sense at all to 'partly' gas anything and leave a large amount of MA freebase behind (especially 1/4oz). I could see someone not bothering pulling the last dregs or leaving a little nonpolar behind if they didn't have a sep funnel and was 'pouring' it off or 'sucking it up but 1/4 oz is something you don't leave behind - not in the normal world. What was his reason for not salting it out? ( Some people can be fuckers and just want to see some tweaker spend 72 hours fucking around with something that isn't going to deliver)....but then the world can be a strange place... maybe someone got busted and they had to stash the NP...
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  #7   Add goodroad to your ignore list  
Old 2007-04-21, 06:12
goodroad goodroad is offline
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Default Re: got someones left overs

your right on the money swihf. thats whats going on besides that swigd thought that this place was here for info not 20million questions if peeps want to know my life story wait for the book. Swigd always comes here for info and gets a great amount of help. but if its a prob. then I'll bounce else where, since it seems that you have something better to do with your time. And if you don't want to answer then why even reply and say anything at all???? Anyway thanks for those of you who have helped out . as far as the shit swigd see's shit floating around looks like snot thats right in the middle where the 2 layers seperate.... any help with this please just want it out of the mix so its out of swigds friends house.
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  #8   Add gigster to your ignore list  
Old 2007-04-21, 07:25
gigster gigster is offline
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Default Re: got someones left overs

you dont supply information to get any answers. So you got a NP solvent so what ,was it from a wash of the post reaction mix? or was it the NP someone based the post reaction honey into?(one gases for the salt no to get freebase) so lets ASSume since you dont tell us its the NP from based reaction honey you got 2 options 1- dry the NP and gas or 2- do a titration.Thats it theres no hocus pocus chant for you to do thats going to magically put MA freebase into that NP solvent .
The snot you see is probably just that the guy that gave you the NP blew it in there so when he tells his educated friends the story they will have a great laugh.
And whos swihf?
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  #9   Add UK_TOM to your ignore list  
Old 2007-04-21, 08:56
UK_TOM UK_TOM is offline
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Default Re: got someones left overs

Was the gas dried throughly? If it is not dry you can get the water content of the HCl gas absorbing the MA and I think that can look apparently, like 'snot' - just go for a titration of the NP - take the Ph straight down to 1 - don't worry about it for now - going for Ph 6 and that is not really necessary - take it to 1 - evapporate the water after you have removed it from the solvent and then if thereis any MA in there it will show up - NB- when swiy is evaporating there will be a nasty HCl gas fumes coming off (they aren't too bad - just don't have a good sniff -e specially if swiy is trying a speedy evaporation on heat). After evaporation take the MA and give it a good acetone wash - this will turn the acetone yellow as it removes the excess HCl acid and returns the MA to a neutral ph. If, there is anything in there it will come out.
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  #10   Add hrsepwrjnky to your ignore list  
Old 2007-04-21, 19:58
hrsepwrjnky hrsepwrjnky is offline
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Cool Re: got someones left overs

Quote:
Originally Posted by goodroad View Post
right now there are two layers swigds friend put dh20 in to the NP so thee are to layers with snot floating around. this was gased once be for to get the free base but before hand was sitting in NP for months.
already added dh2o? easy way would be to add mur acid few drops at a time,swirling between drops,until ph of water layer is a 7,then drain off water layer and let dry,if there is anything there that should get it out.swiwpcc thinks your being fed full of shit,but there's your answer.
peace out swihpj
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This thread continued for 3 pages in the real archive, 26 posts total - only page 1 survived here.
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