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Laboratory Tips Safety proceedures, test reagents, drilling rubber stoppers, bending glass tubes, etc. Contributed to by chemists.

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 #1 
Old 2004-01-20, 22:03
stillbill stillbill is offline
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Default ? for Jam or Wicked Rain.

Taking note of the last post WR sent back to me about the dryness of the precursors(using

sieve to ensure the dryness of rp and pseudo). Swis usually adds 1 ml. of dh2o per gram of pseudo to the mix generally with good results. Swis has always been told to do this or the rxn would be way to dry doing the short hot cook. Highest temp. around 185

degrees F. My question is this proper as Swis has always been told to do this? Just trying to make rxn better unless you guys see some

oversight in my method. Btw, swis always ensures I2 crystals are as dry as possible

before adding to the mix. Cook time is about

7 to 8 hours. Any added info would be greatly appreciated! As always, Thanks!
 #2 
Old 2004-01-20, 22:34
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Default Re: ? for Jam or Wicked Rain.

1mlper gram is perfect.

185F is debatable by many...but I've tinkerd with the temps myself and unless you got a heating mantle the heat is in fluctuations .

So all this business about IT HAS TO BE 205C OR ITS FUCKED IS RUBBISH!!

Get fucking real I say!!



In short, if this is how its been done I seee nothing broken here....and if it ain't broke then ????



If it gets kicked up to 200 itis A-Ok.

THERE IS NO ONE TEMP TO USE!!

Remember that Bro.

Do't pay no attention to the noise as it gets loud t times!! lol!!

Just wash your polar and non-polars with the other and with it hot as can get!!!

The impurities will for the most part follow.

This is a most important virtue.

The temp and H2O saturation rates to the precursors are really however you find you fancy them to be.



Just keep that 185F the lowest the bottom of that flask is going to go.



Jam.

[This message has been edited by Jamiroquai (edited 01-20-2004).]
 #3 
Old 2004-01-20, 22:45
stillbill stillbill is offline
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Default Re: ? for Jam or Wicked Rain.

Thanks, Jam. Maybe I was just looking for something I was unaware of, but for the most part, everything has been turning out fine.

One thing I wasn't aware of was the hot polar and nonpolar. Will make sure this is done in the future! Many thanks again, Jam

Peace
 #4 
Old 2004-01-21, 01:05
Wicked_Rain Wicked_Rain is offline
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Default Re: ? for Jam or Wicked Rain.

Jam & SWIM went to different fuckin schools together it seems lol. SWIM agrees with Jam 100% here. SWIM runs his about 190 degrees and uses 0.7 ml of DH2O. SWIM usually shoots for 12 hours but has had to hustle it at 4 or 5 hours with good results. so way SWIM sees it your right on the money bud. those NP washs of the rxn fluid and water washs of the NP are the difference tween great results and excellent results. people dont grasp how much this does for the goods.the shit can be killer and the washs dont really make the shit better as in longer legs more rush etc. but what it removes makes the side effects much more bearable. its kind of hard to explain. but washing will make you king of the hill. SWIM does know that the main reason cooks fear the wash is inexperience. they are afreaid of fuckin up and losing product. but its just not possible. you can wash the rxn fluid 1000 times with a 100 gallons of NP and as long as the rxn fluid hasnt been based you CANNOT lose a single molecule of dope not one. its just not possible. same go`s for water washing the NP after the A/B. once its in the NP it will not migrate back to the water, period. there are no meth molecules that stuck in the middle lol
 #5 
Old 2004-01-21, 01:24
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Default Re: ? for Jam or Wicked Rain.

Wicked I'd like to buy you a beer!! <A HREF="http://techhelpers.net/e4u/drink/trink39.gif">http://techhelpers.net/e4u/drink/trink39.gif" width="90" height="90 (http://techhelpers.net/e4u/drink/trink39.gif" width="90" height="90)</A>



I see the Old-School in you more and more man. Not to say I doubted it before now....just saying it shows itself in honest ways.

I would buy you a beer and burn a joint with you anytime Bro.



Jam.
 #6 
Old 2004-01-21, 02:02
stillbill stillbill is offline
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Default Re: ? for Jam or Wicked Rain.

Thanks again to the both you!!
 
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