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Laboratory Tips Safety proceedures, test reagents, drilling rubber stoppers, bending glass tubes, etc. Contributed to by chemists.

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 #1 
Old 2004-01-12, 15:37
amine_assimilator amine_assimilator is offline
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Default how wet?

SWIM knows there is a range of amounts of dH2O that can b used in a synth.

let's say SWIM is looking for a scalable formula. would half a ml. per gm. of pseudo b appropriate for a 24hr. cook? SWIM's precursors are pretty well dried.
 #2 
Old 2004-01-12, 15:53
kirby kirby is offline
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Default Re: how wet?

how wet you ask,

they say you must get them as wet as possible.
 #3 
Old 2004-01-12, 16:13
amine_assimilator amine_assimilator is offline
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Default Re: how wet?

that applies to pussy, kirb, not a m synth, as i'm sure u know.



SWIM has no problem w/ the pussy, but how much water for the RXN?
 #4 
Old 2004-01-12, 17:33
kirby kirby is offline
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Default Re: how wet?

buggered if i know,,i birch,,

a few of the other lads will be on soon,,

theyl answer
 #5 
Old 2004-01-12, 18:30
kman kman is offline
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Default Re: how wet?

Swim thinks that might be a little dry for 24 hours.
 #6 
Old 2004-01-12, 23:19
amine_assimilator amine_assimilator is offline
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Default Re: how wet?

hmm, but a ml. of dH2O per gm. of pseudo would b too much, right? SWIM knows the h2o amount is somewhat personal, but what would b a good amount whilst providing the greatest safety margin (SWIM's still too noobyish to feel 100% confident).

SWIM would like to also ask about fellow dreamer's cook time recomendations but knows this topic is even more hotly disputed, which is why SWIM settled on 24 hr.s.
 #7 
Old 2004-01-12, 23:23
kman kman is offline
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Default Re: how wet?

Swim's never dreamt of one that long, but would guess in the 0.6 to 0.8 range. If it's too dry, you can always add a little water.
 #8 
Old 2004-01-12, 23:41
amine_assimilator amine_assimilator is offline
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Default Re: how wet?

thanx, kman. to add water later on SWIM should use a syringe in the condenser tubing followed by tape, lest the HI escape, correct? or is there really much HI left at that point anyway?
 #9 
Old 2004-01-12, 23:53
madchemist madchemist is offline
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Default Re: how wet?

Start off with a half of a milliliter, then add more if you need to. SWIM always used to do this synth with a balloon. If he needed to add more water, he would just twist up the balloon and clamp it with hemo's. Then remove it, add the water and replace. Sure some HI would escape, but so what?
 #10 
Old 2004-01-12, 23:59
amine_assimilator amine_assimilator is offline
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Default Re: how wet?

kewl deal. first dream flucked by stupid mechanical, not chemical mishap.



tommorow SWIM attacks anew.

no prisoners.

victory at all costs.
 
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