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| Laboratory Tips Safety proceedures, test reagents, drilling rubber stoppers, bending glass tubes, etc. Contributed to by chemists. |
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#1
 2004-01-07, 06:43
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Cichlid 
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Copper (Still) Reflux condenser
Ok,
So I'm a little clumbsy and glass and me don't seem to get along too well I've been wondering if I can build a reflux condenser using copper pipe and fittings etc. Will the copper taint the reaction/end product?
Any help
[This message has been edited by Cichlid (edited 01-07-2004).]
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#2
 2004-01-07, 07:23
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kirby 
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Re: Copper (Still) Reflux condenser
i dont know,,,
what i do know is copper and solvents dont go together
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#3
 2004-01-07, 08:34
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Wicked_Rain 
Regular
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Re: Copper (Still) Reflux condenser
if your talking about using a copper condenser in a RP/I2 rxn the answer is no. hydriotic acid eats metals.
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#4
 2004-01-07, 08:58
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kman 
Regular
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Re: Copper (Still) Reflux condenser
If you're a little clumsy, maybe you shouldn't be fooling around with dangerous things!
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#5
 2004-01-17, 04:06
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wthswtthighs 
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Re: Copper (Still) Reflux condenser
PVC pipes
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#6
 2004-01-17, 04:20
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Re: Copper (Still) Reflux condenser
quote:I've been wondering if I can build a reflux condenser using copper pipe and fittings etc.No.
quote:Will the copper taint the reaction/end product?
Yes.
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#7
 2004-01-17, 04:31
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Speddy Eddy 
Regular
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Re: Copper (Still) Reflux condenser
quote:Originally posted by wthswtthighs:
PVC pipes
Thats a complete no no!
Im pretty sure that both polar and non-polar solvants will disolve PVC which will contaminate your end product so remember...
Solvents + PVC = very bad!!!
[This message has been edited by Speddy Eddy (edited 01-17-2004).]
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#8
 2004-01-17, 17:44
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Re: Copper (Still) Reflux condenser
quote:Originally posted by smitty:
I have read somewhere where impure 'end use" solvents(eg. toluene) may be responsible for a product that goes totally oily in plastic after just a short time, and doesnt recrystalize under normal conditions of temp., etc. This is from a rpi method op. Excuse my obvious lack of knowledge on the guts of the subject, I'm just asking for a friend (he does the bomb, consistently...but methodology falls into the "mad genius" category...wild..
quote:Originally posted by Speddy Eddy:
Dude,take that shit to lab tips,we know fuck all about the synthesis of drugs.
quote:Originally posted by Speddy Eddy:
Dude,take that shit to lab tips,we know fuck all about the synthesis of drugs.
you're a fucking idiot. dont speak for us.
quote:Originally posted by wthswtthighs:
PVC pipes
Thats a complete no no!
Im pretty sure that both polar and non-polar solvants will disolve PVC which will contaminate your end product so remember...
Solvents + PVC = very bad!!!
What the fuck Speedy Eddy?! Do you suffer from multiple personality disorder?!
Jam. <A HREF="http://users.telenet.be/eforum/emoticons4u/violent/sterb157.gif">http://users.telenet.be/eforum/emoticons4u/violent/sterb157.gif" width="90" height="90 (http://users.telenet.be/eforum/emoticons4u/violent/sterb157.gif" width="90" height="90)</A>
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#9
 2004-01-17, 17:49
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Re: Copper (Still) Reflux condenser
All originally posted here.
http://www.totse.com/bbs/Forum26/HTML/003585.html
http://www.totse.com/bbs/Forum26/HTML/003547.html
Jam. <A HREF="http://users.telenet.be/eforum/emoticons4u/violent/sterb090.gif">http://users.telenet.be/eforum/emoticons4u/violent/sterb090.gif" width="90" height="90 (http://users.telenet.be/eforum/emoticons4u/violent/sterb090.gif" width="90" height="90)</A>
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#10
 2004-01-17, 20:13
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Speddy Eddy 
Regular
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Re: Copper (Still) Reflux condenser
<A HREF="http://users.pandora.be/eforum/emoticons4u/crazy/1076.gif">http://users.pandora.be/eforum/emoticons4u/crazy/1076.gif" width="90" height="90 (http://users.pandora.be/eforum/emoticons4u/crazy/1076.gif" width="90" height="90)</A>
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#11
 2004-01-18, 03:38
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tryptamine 
Regular
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Re: Copper (Still) Reflux condenser
The only thing you can use with acids is glass, you can use a copper reflux still with solvents and such. Kirby, what kinds of solvents don't go with copper?
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