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| Laboratory Tips Safety proceedures, test reagents, drilling rubber stoppers, bending glass tubes, etc. Contributed to by chemists. |
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#1
 2003-12-28, 09:56
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wrong_way 
Regular
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no blue in pseudo
swim is attepmpting the TCE/JD method for his pseudo. swim is following as he should with no substitutions in chems. he got as far as filtering the tce and jd out of the pill mass and letting it dry. he has read that there should be a blueish greyish tint, but it has dryed and there is no blue. he was eyeballing the amounts of chems to use up to this point. was this the problem? what did he use too much or too little of? can he fix the problem if there is one w/o starting over? thankyou.
[This message has been edited by wrong_way (edited 12-28-2003).]
[This message has been edited by wrong_way (edited 12-28-2003).]
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#2
 2003-12-28, 11:36
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kirby 
Regular
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Re: no blue in pseudo
before flapping your gums,
wait to see how much you have..
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#3
 2003-12-28, 20:06
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sitbcknchill 
Regular
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Re: no blue in pseudo
its not always real apparent but keep on goin and see what ya got then come back and ask where u fucked up....when its dry you cant really see alot of blue...when you get it wet again you'll see the diff
[This message has been edited by sitbcknchill (edited 12-28-2003).]
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#4
 2003-12-28, 20:24
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kman 
Regular
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Re: no blue in pseudo
Maybe you got lucky and nothing was left behind, but I doubt it. Swim's noticed the blue color after the powder is completely dry, not when it was wet, but I guess different stuff would show up at different times. Did you rinse with dry acetone? The only solution I can see was if your pills were very clean, with very few inactives. What were the actives and inactives?
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#5
 2003-12-28, 22:26
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wrong_way 
Regular
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Re: no blue in pseudo
Active
Ephedrine HCL .60mg
triplidine 2.5mg
Inactive
methylcellulose
lactose
magnesium stearate
polyethylene glycol
starch
stearic acid
titanium dioxide
no i haven't made it to the acetone wash yet. once i filtered and i didnt think it looked the way it was supposed to i automatically assumed i messed up and stoppped there. i didn't want to continue if i did something wrong and there was a way to fix it. i guess i'll just continue though. thanks for your feedback, it was much appreciated.
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#6
 2003-12-29, 03:49
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kneedragger 
Regular
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Re: no blue in pseudo
#1) was there a blue tint at all when the seudo was dissolved in D. Alky?
#2) If it was blue in the alky, how long did you let the p-fed dry?
--kneedragger
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#7
 2003-12-29, 08:47
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wrong_way 
Regular
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Re: no blue in pseudo
the d. alky hasn't touched the pill mass yet. i stopped the extraction after filtering the brake kleener and the japan dryer off and thought the color wasn't quite right. i'm thinking that maybe i was just expecting more of a blue to it than there was. i'm going to assume that everything is ok and continue. i'll let ya'll know how it turns out.
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#8
 2003-12-29, 09:06
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BorisB73 
Regular
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Re: no blue in pseudo
SWIB tried the TCE/Jd method yesterday. His first crystals after the soak were slightly greyish-blue. After the alcohol pulls, his crystals were greenish-blue... still confident... after the acetone wash the crystals came white... score.
Try working to the end of the procedure... SWIB thinks not all japan dryers may be made equal... The pseudoephedrine pills can be different too...
And, Kirby, if you catch this - Excuse my ignorance in asking about the Eph. I wasn't putting two and two together and just blurted out my retarted Eph question...
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#9
 2003-12-30, 02:16
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kman 
Regular
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Re: no blue in pseudo
Swim dreams of running dry acetone through the pseudo after the TCE/JD, until the blue is gone, because he heard this was the way to go.
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#10
 2003-12-30, 03:42
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kirby 
Regular
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Re: no blue in pseudo
ok boris,
sorry about my response to,
sometimes my impatience strays into my answers...
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#11
 2003-12-30, 03:53
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sitbcknchill 
Regular
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Re: no blue in pseudo
ive noticed that in the last couple of your posts kirby...you need some sleep or sumthin man... 
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#12
 2003-12-30, 05:53
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Wicked_Rain 
Regular
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Re: no blue in pseudo
wrongway,
carry on with the method you are on course with no worries. the list of actives & inactives you gave tells SWIM that you are doing ok. the blue color comes from the trip 2.5 mg. sometimes its slate blue almost a light grey sometimes its really blue, the color varies. follow the technique thru to the end and you will have some pristene snow white psuedo. SWIM knows this to be fact by the list you provided above. its all good.
[This message has been edited by Wicked_Rain (edited 12-30-2003).]
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#13
 2003-12-30, 06:03
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kirby 
Regular
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Re: no blue in pseudo
hi chill
it isnt sleep mate,
its the heat down here in the west,
it never ends,
now add 3 children,
an annoying constabulary,
and a growing sexual attraction to my airconditioner,
and all that seems to turn into intolerance on my behalf..
bare with me guys,,only 5 more months of ripyourarseoutheat..
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#14
 2003-12-30, 06:09
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Wicked_Rain 
Regular
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Re: no blue in pseudo
its a balmy 33 degrees below zero F. here where SWIM hangs his hat. SWIM see`s about 9 feet of snow on the ground when he looks across the land will prolly drop another 9 feet by april. such is life in the far north. SWIM loves it.
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#15
 2003-12-30, 06:22
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sitbcknchill 
Regular
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Re: no blue in pseudo
kirby swim dont blame you swim would proly flip shit to...he cant complain though its been in the 50's here so its not to bad...he just got done with a snow storm last week though...swim would rather freeze his ass off than melt anyday
bet you love to go to work though...for more than one reason
[This message has been edited by sitbcknchill (edited 12-30-2003).]
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#16
 2003-12-30, 06:58
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kman 
Regular
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Re: no blue in pseudo
I feel ya, Kirb, I hate the heat! I got 5 inches of snow yesterday, my mom got 16 inches of snow yesterday, and my hometown got 4 feet. I love the snow!
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#17
 2003-12-30, 08:17
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kirby 
Regular
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Re: no blue in pseudo
your moms a lucky girl getting 16 inches yesterday
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#18
 2003-12-30, 08:35
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kisme_t 
Regular
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Re: no blue in pseudo
^^^^^ "MOM"??????!!!!!!!
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#19
 2003-12-30, 09:56
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kirby 
Regular
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Re: no blue in pseudo
no kismet,
not your mother,
we know she wouldnt be copping 16 inches,
of snow..
might cop 16 inches of crabs though..
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#20
 2003-12-30, 19:57
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sitbcknchill 
Regular
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Re: no blue in pseudo
lolololololol sry i had to laugh
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