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Laboratory Tips Safety proceedures, test reagents, drilling rubber stoppers, bending glass tubes, etc. Contributed to by chemists.

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 #1 
Old 2003-12-28, 04:06
sitbcknchill sitbcknchill is offline
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did up about 200 and some odd pills...lost count. they were 60's from dg...ground up pills and run through fine seive strainer twice to make sure it was very fine...mixed up his beet juice and poured over pm. stirred then let sit for proly a minute...filtered...proly took about 2 minutes maybe a little more...let dry till it was bone dry...passed through seive...put in jar and added about 250ml da let set an hour decanted and filtered with one filter and charmin plug then evapped...did this two more times.... first evapp got gakked and second and third are still evaporating but it doesnt look good....swim dont understand why he was gakked cause the last couple he did turned out fine....and he did the same thing....but he did notice that after the da pm sat an hour it was still cloudy...when he saw how cloudy it was he had his suspicions but he evapped anyway to see if it would be ok but it wasnt

[This message has been edited by sitbcknchill (edited 12-28-2003).]

[This message has been edited by sitbcknchill (edited 12-28-2003).]
 #2 
Old 2003-12-28, 04:43
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Keep filtering and maybe including a cotton balled-tip in the funnel(don't make it tight nor loose just kinda fit in there and you can test it by sucking air through the tip of the funnel, you want it to where air draws with relative ease yet when you shine it at a light no sign of that light shines through).

Be sure to prewet your filters of course as well as your cotton balls and pour the liquidthrough until there isn't a hint of cloudiness.

That cloudiness is telling you that there are free-radicals so-to-speak still attatched to the pseudo and they will eventually filter out.

Also, use the biggest funnel possible and add-on more filters the filtration-system at hand.

Remember this man. You must have at any stop in this train-ride to methville.......you must have your liquids clear as a bell before moving on to the next step.

Same thing when you finish a batch and are filtering out the post-reaction fluid. Filter it out until clear.

This will give you a much more proper product.

And don't think that there aren't us who like you will have to, that we don't have tofilter shit sometimes twenty-five-million-fucking times before the fucker goes clear!!!



Nobody escapes from this all the time.

So clear means go!!------>

Cloudy means STOP!!



There are no in betweens here or yellow lights.

Just Redlights and Greenlights man.

Okie dokie?!



Jam.
 #3 
Old 2003-12-28, 04:51
sitbcknchill sitbcknchill is offline
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Default Re: E

thx jam...thats what my problem was cause the da never became clear sitting ontop the pill mass...i would filter and it would still be a little cloudy...now swim will filter a couple times or a million before evap instead of once



by the way swim took his crap and poured acetone over it and the crystals dropped out and tone turned light blue like it supposed too...what swim was wondering is can he redo his da pulls with what he has now?

[This message has been edited by sitbcknchill (edited 12-28-2003).]

[This message has been edited by sitbcknchill (edited 12-28-2003).]
 #4 
Old 2003-12-28, 05:10
Regular
 
Default Re: E

Yeah no problem. There isn't anything in there that can't be sorted out.



Just resume as normal and good luck and Happy Dreaming.



Jam.
 #5 
Old 2004-02-11, 05:27
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Default Re: E

Nobody escapes from this all the time.

So clear means go!!------>

Cloudy means STOP!!



There are no inbetweens here or yellow lights.

Just Redlights and Greenlights man. <A HREF="http://techhelpers.net/e4u/drink/trink13.gif">http://techhelpers.net/e4u/drink/trink13.gif" width="90" height="90 (http://techhelpers.net/e4u/drink/trink13.gif" width="90" height="90)</A>



Jam
 #6 
Old 2004-02-11, 12:29
sitbcknchill sitbcknchill is offline
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Default Re: E

yeah that is so right

jam what did you do get bored



..and what happened to the purples and the blues



[This message has been edited by sitbcknchill (edited 02-11-2004).]
 #7 
Old 2004-02-11, 12:41
kirby kirby is offline
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Default Re: E

you dried your solvents didnt you
 #8 
Old 2004-02-11, 19:23
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No. Sulfates scare me.
 
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