|
|
 |
 |
 |
 |
register |
bbs |
search |
rss |
faq |
about
|
 |
 |
meet up |
add to del.icio.us |
digg it
|
 |
 |
| Laboratory Tips Safety proceedures, test reagents, drilling rubber stoppers, bending glass tubes, etc. Contributed to by chemists. |
 |
|
|
#1
 2003-12-21, 16:22
|
amine_assimilator 
Regular
|
|
|
|
where'd it go, why does it sting and, what is it?
SWIM recently had an extremely flooded synth that happend bfore the initial reaction took place; this was bcause of a RP fire and a broken flask.
rather than boil it down to try to refire it, SWIM chose to do a normal honey workup to reclaim the pseudo (didn't want to wait for all that H2O to go).
now, SWIM would've gotten 2.5gm. of M at 50% return on the pseudo if, the RXN had compleated, but from the honey's first and second pulls (still waiting for the third) SWIM only got 1.1gm back.
question time:
1. where did it go? SWIM isn't expecting much more from the third pull so, could the RP fire in the flask (bfore it cracked and flooded) have burnt away the missing pseudo and/or could it b all that H2O SWIM had to deal with?
2. the resulting pseudo Hcl SWIM got was crashed, washed and flashed w/ dry cold 'tone, yet the pseudo burnt SWIM's nostrils when SWIM tried a couple of key sized bumps (just to experiment). is there remaining acid? SWIM thought he 'toned it well, will more help?
3. what is it? it should b only pseudo Hcl but, even though the key bumps burned (SWIM had to flush nose w/ water seconds after huffing them) the effects were more enjoyable than a couple of sue the feds would b. the reaction did take place for a min or two bfore the RP fire and flask mishap and the flooded (250ml H2O) RXN was left at room temp w/ cond. attached for 5 days (cold reaction?)
could a small amount have been converted to meth and/or ido/ iodo compounds?
4. this Hcl, b it pseudo or, whatever; can it b added to a new synth? at what ratio? can SWIM mix it w/ pseudo freebase in a synth?
|
|
#2
 2003-12-21, 17:04
|
|
|
Re: where'd it go, why does it sting and, what is it?
a_a you are not doing too shabby considering the trauma your half/precursors/half reduced prcursorsendured and went through.
Sounds like you got some acidity there.
Do you have PH-strips there that go to black(14)?
And asolutley the pseudo was getting stripped down andmolecule by molecule was doing so when the five-alarm fire broke out.
If you enjoy the buzz, then it's your call as to if you keep the honey you have crystalized.
Otherwise, throw the rest into the next reaction and you'll have just that much more weight to pull next time you are basing and acidifying the freebase to crystaline salt creations. <A HREF="http://www.salacious.de/Smiliez/Gefuehle/Gluecklich/Winken/winken490.gif">http://www.salacious.de/Smiliez/Gefuehle/Gluecklich/Winken/winken490.gif" width="90" height="90 (http://www.salacious.de/Smiliez/Gefuehle/Gluecklich/Winken/winken490.gif" width="90" height="90)</A>
I guarntee you this man. You have learned alot here by what has happened and I know next time we will be getting a positive report of how the pseudo freebase reduced down to some of the best damndest dope you have ever consumed!! <A HREF="http://emoticons4u.informationalot.com/cool/049.gif">http://emoticons4u.informationalot.com/cool/049.gif" width="90" height="90 (http://emoticons4u.informationalot.com/cool/049.gif" width="90" height="90)</A> Smoke a bowl of it and see if you tip of your ongue tastes the acidity that's where the recptors are for that particular sense of taste.
Jam.
|
|
#3
 2003-12-21, 23:17
|
Wicked_Rain 
Regular
|
|
|
|
Re: where'd it go, why does it sting and, what is it?
where did it go?
a penalty invoked by the meth-gods.
|
|
#4
 2003-12-21, 23:30
|
|
|
Re: where'd it go, why does it sting and, what is it?
Yes.
But you now have paid the price of learning and will be left aloe provided you pay attention. hehe...
Soon you won't be able to mess-up if you were doing it in your sleep.
This is where folks get aggrevated by others asking for things they must with their own brains and their own bodies, go through the motions we all in the beginning had to go through and live and ulitmatley learn.
Had you not of cracked that flask you would have earned you a pile full of pleasure and cherished treasure.
There is however, always next time.
Minus possible hostile foreign objects better left outside the flask and maybe in the trash.
Most go through the reaction and end-up with wishfull thinking their first time or ten.
I'd say because of iodine crude and unrefined and way to wet to ever expect to create and recycle HI when mixed with R.P.
Have you heard of the lonesome loser?!
He's a loser but he still keeps on trying!!--Little River Band.
Jam.
|
|
#5
 2003-12-22, 05:18
|
amine_assimilator 
Regular
|
|
|
|
Re: where'd it go, why does it sting and, what is it?
hey Jam, how's it hangin'? thanx for the support and faith. SWIM is still kicking his self for the garbage in the flask scenario and is confident he had slammin' precursors that went to naught.
next time SWIM takes no prisoners!
victory at all costs!
so, could there really b much M in that Hcl SWIM reclaimed from the failure?
would more cold dry 'tone help w/ the acidity of the reclaimed Hcl or does it call for a recrystalization?
so a glass stem/crack pipe is OK for toking?
and, yes, Jam, SWIM has learned alot from the mishap. SWIM viewed it as a chance to practice honey workup, seperatory funnel technique, precursor reclaimation, etc. u know, silver lining and such.
praise b to TOTSE, you are a terrific site!
SWIM had known about Lyceum, Rhodium, Erowid, etc. for a long time and had always wanted to try a M RXN but thought it too technical, upon happening unto TOTSE SWIM knows it's possible.
SWIM hopes to have product for new year's eve, meth gods willing.
|
|
#6
 2003-12-22, 20:40
|
kman 
Regular
|
|
|
|
Re: where'd it go, why does it sting and, what is it?
Your RP caught on fire? I've never seen that before!
|
|
#7
 2003-12-23, 06:19
|
|
|
Re: where'd it go, why does it sting and, what is it?
"Your RP caught on fire? I've never seen that before!"
Me neither, and hopefully never will. ahahaha I've read a little about stupid mistakes...over at the hive, Rp fires are some of the worst! (if say your flask shattered while it was going) But we all know the right precautions to take ehh??
*puts on safety glasses, and brings in 5 gallon bucket of moist potting soil, and wet beach towel*
|
|
 |
 |
To the best of our knowledge, the text on this page may be freely reproduced and distributed.

totse.com certificate signatures
|
 |
 |
About | Community | Bad Ideas | Drugs | Ego | Erotica | Fringe | Society | Technology
|
 |
 |
 |
 |
|
|