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| Laboratory Tips Safety proceedures, test reagents, drilling rubber stoppers, bending glass tubes, etc. Contributed to by chemists. |
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# 1

2003-12-21, 08:41
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tried again wicked's method and got no clean anything. followed it too the t and got shit. someone tell me what the fuck i am doing wrong. or what other method works. using the rp/i method and have a good grip on how it works. cant get the damn pills clean now. argh!!! using 25mg psuedohcl pills. easist to get, esp w/ the flu season. cant get any of the dollar store 30's and 60's. guyz give me some help here. u all are the brains and soo helpful soo far. been on rhodiums site for last few days and rsched some more. like i said got hte method pretty well down pat from trying but now cant get the pills to clean. used acetone in the microwave once but was told that was not the way either. had about 700 p30 mg pills and covered in acetone and baked in mic. got crystals but was told that was nooo good by friend who does annie. want too be able to make this work and enjoy in front of bf who dont belive i can make it work. well also tired of being dicked around by these people who have it.
thanks u guyz and girls
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# 2

2003-12-21, 09:04
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down there
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hi miss
wickeds tce/japdrier does work,,
and untill you post what you did step by step then we cant help you..
but
if your using the 25mg little white pills,,not over the counter sinus and congestant pills,,
try giving them 2 dry acetone washes,,
3 alky extractions
crystalize your eph
an A/B
thats all you need
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# 3

2003-12-21, 09:24
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Quote:
quote:Originally posted by kirby:
hi miss
wickeds tce/japdrier does work,,
and untill you post what you did step by step then we cant help you..
but
if your using the 25mg little white pills,,not over the counter sinus and congestant pills,,
try giving them 2 dry acetone washes,,
3 alky extractions
crystalize your eph
an A/B
thats all you need
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kirby - thanx for the quick response man.
had 360 25mg hcl pills. extraction fluid was 280 ml iso, 280 ml vmp naptha, 8gm salt, 16mg epsom. let sit 15 mins cause still reacting after 10 mins. poured off all but solids. added 1/3 to piills. boiled on med high heat. filtered off. repeated 2 more times. added 200ml xylene to the fluid. boiled to 105C and then funneled off. nothing in the filter. help me kirby. where have i gone astray.
in the method u mention. sorry for the ignorance but plse be more specific on the alkyl portion . understand the rest implicitly.
thanx kirby for the response. swim will be dreaming agian soon, bc swim is tenacious.
g'day mate!
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# 4

2003-12-21, 11:00
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down there
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well the whole procedure is wrong..
the iso is your extraction solvent..
you add that to naptha
boil and filter x3
you pulled the eph with the iso,,
then the 3 boils evaporated the iso,, putting the eph back into the pill mass..
one hopes you havent chucked the pill mass...
wash the pill mass in 600ml of zylene for 5mins at 105c..
chuck zylene..
allow pill mass to cool..
wash pill mass x 3 with 200ml of dry iso each time..
filter iso with 3 filters and cotton wool balls stuffed into the funnel stem...
evaporate the iso slowly..
youll see your ephedrine then..
you display a rare talent miss...
the willingness to get in there and get your hands dirty...
choose your husband wisely..
the wrong one may open roads that lead to a cell with a massive 300 pound lesbian who grins when she sees you
[This message has been edited by kirby (edited 12-21-2003).]
[This message has been edited by kirby (edited 12-21-2003).]
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# 5

2003-12-21, 12:54
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another thing is you keep tellin us that the only pills you can get are 25 mg ephedrine etc. well we know they have eph. in them. why not try telling us what the INACTIVES are. no one cares to hear about the eph. cuz we know that they have that as the active already or you wouldnt be buying them. the only 25 mg eph. HCL pills SWIM has ever seen are mini-thins and the like. SWIM has never seen 25 mg. cold, sinus, or allergy pills in the usa. if the pills have gauf. or caffiene in them then they are fucked. and one last thing, quit saying you are using wickeds method and following it to a tee etc. what you typed up ^^^ there is most certainly not anything wicked has ever done in any form or fashion. what you say you did in your post wouldnt extract eph if it was pure. so buckle down, follow the write up EXACTLY as written with NO substitutions. travel untill you find the proper shit. when SWIM leaves to fill a supply list he dont come back home untill its filled. he dont care if he has to drive 500 miles. simple as that. cost up front compared to return makes it worth every effort and then some even if you dont sell the shit and do it all your self what you save in cash trying to buy the same amount not to mention the street shit you buy aint worth a fuck most times lol. remember, where it ends just depends on where you start.
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# 6

2003-12-21, 15:02
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tce/japan dryer does work.....take into account first method swim ever used first time swim tried it, got it right...it REALLY isnt that hard...but u HAVE TO FOLLOW INSTRUCTIONS...and swim can prolly say it kickes the shit out of cookin it but like he said he wouldnt know.....
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# 7

2003-12-21, 15:28
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The 25mg eph. thing has swim confused also. The ones swim gets are 30's no other active, and 60's has 4mg maleate?on spelling.
Here is a guick tip swim has found useful when shopping for cold and allergy med.
30's------> Red & White box
60's------> Green & White
120's-----> Blue & White
240's-----> Yel & White
W.W., D.G., Wgn. brands ect are like this. Also check the grocery stores they all usually care the same. It makes it alot easier to know your boxes by sight instead of having to stand there and read them.
Princess
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# 8

2003-12-21, 19:36
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Doesnt anyone here know how to use paragraphs and punctuation?
Anyway!
Instead of starting a new thread about psuedo extraction I'll post in here.
Is there a suitable substitute for Isopropyl Alcohol? I cant find rubbing alcohol anywhere...
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# 9

2003-12-21, 19:51
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down there
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you come in here and criticise members on there grammar,,
then ask these same members for advice.
heres some advice;
dont criticize needlessly,those whom you need.
and yes,,
theres quite a few,,
and i dont think rubbing alcohol is one,,
doesnt it have an oil additive??
try methanol..
what country are you in
as there are quite a few you could use but each country uses different names
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# 10

2003-12-21, 19:59
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Just seems near impossible to read without paragraphs. Sorry about being rude..
Im in the UK.
I thought that if you got your hands on about 99% rubbing alcohol you had near enough pure Isopropyl.
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#11
 2003-12-21, 20:01
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Re: cleaning psuedo hcl 25mg
Agreed.
Does the U.K. sell pure grain alcohol(190-proof/95% ethyl alcohol).
If so use it.
It is the ultimate fuel and the ultimate alcohol in my book.
I brew mine.(rye-based for drinking and molasses-based for my 427-1970-Hemi-Cuda)<-road-ripping-fun I tell ya!!!
Jam.
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#12
 2003-12-21, 20:49
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kirby 
Regular
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Re: cleaning psuedo hcl 25mg
jam is correct
as usual
try finding anything but methanol,,
use it as a last resort..
methylated spirits can be used as the very last resort
but dry it
jam
did you say rubbing alcohol was fine to use?
[This message has been edited by kirby (edited 12-21-2003).]
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#13
 2003-12-21, 23:03
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Wicked_Rain 
Regular
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Re: cleaning psuedo hcl 25mg
SWIM dont puncuate. SWIM dont use correct grammer. SWIM dont give a fuck. but SWIM is an extracting motherfucker jack heh. WORD!!!!
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#14
 2003-12-21, 23:07
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BorisB73 
Regular
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Re: cleaning psuedo hcl 25mg
So either Denatured alcohol or Isopropyl alcohol can be used for the decanting?
Jam stated somewhere that half the trouble with the online learning is deciphering the messages people send. I can't agree more! It's been tough, but I'm finally getting it... I think...
[This message has been edited by BorisB73 (edited 12-21-2003).]
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#15
 2003-12-22, 00:19
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Son of Northern Darkness 
Regular
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Re: cleaning psuedo hcl 25mg
I was thinking maybe distilling vodka for the ethanol. Would this work? It's a little pricy but might work.
What do you mean 'dry' meth spirit?
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#16
 2003-12-23, 18:48
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kman 
Regular
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Re: cleaning psuedo hcl 25mg
Squirrelyone, I tried to answer your emails, but got a message that your email addy wasn't working.
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#17
 2003-12-23, 19:40
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Infosponge 
Regular
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Re: cleaning psuedo hcl 25mg
yeah...how do you dry meth spirits? (are we talking about the liquid purple stuff - denatured alcohol?)
Curbshot's effi extraction uses methylated spirits only anyway...
works!!!
why do much more?
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#18
 2003-12-24, 06:17
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kman 
Regular
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Re: cleaning psuedo hcl 25mg
Denatured alcohol isn't purple, so whatever you're talking about must have something else in it-maybe like aromatic hydrocarbons.
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#19
 2003-12-24, 06:49
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squirrelyone 
Regular
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Re: cleaning psuedo hcl 25mg
hello again one and all. before i go on - happy holidays to everyone!!!
swim tried again to clean 30's x 196 and 120's x 30. again swim mixed 210ml iso, 210 naptha, 6gm salt, 12gm iso. brought to boiling, poured off hot. repeated two more times. added 150ml xylene to extraction fluid. swim boiled to 80 degrees C. could not get any hotter according to my thermometer. there was nothing there, but rinsed with MEK anyway in hopes that something would appear. came up empty. im not trying to be a problem here i just cannot figure out why this will not work. is there another method u can point me to to try?!?!? swim wants to see snow for xmas!!!
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#20
 2003-12-24, 07:40
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Wicked_Rain 
Regular
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Re: cleaning psuedo hcl 25mg
Infosponge, curbshots method is outdated and will NOT remove orange gakk 2. you must understand that what worked last year, last month, hell last week may not work today. the pill formulas are constantly evolving in the governments so called "war on drugs" the simple alky extractions of the past are GONE forever, say the eulogy have the fuckin funeral and call it good then start researching here and different sites and be on the cutting edge of extraction tech.
Japan drier is purple.
Squirrly one that method you are using wont extract shit im sorry to say. it sounds like a confuckle of a couple different extractions mixed together. whatever it is it sure isnt wickeds lol SWIM thinks its some bastardized version of the straight to E by video editor. anyways here is what SWIM does, follow the directions to a letter DONT CHANGE ANYTHING AND DONT SUBSTITUTE ANY CHEMS PERIOD!!!! it has worked for literally hundreds of people. the only people that reported probs were people that cant or wont follow simple directions. its easy as hell to follow and you dont have to boil solvents. anyone that cant do this extraction method should give up and get a job and buy there dope.
here the shit is:
*** Neither the author of this post, nor this website or its owners advocate the use, manufacture or sale of any controlled substance. All posts are for information and entertainment purposes only, and should not be considered meaningful. ***
Chems Needed:
TCE= available at your local auto parts store. ingrediants are:
Tetrachloroethylene 127-18-4 & carbon dioxide 124-38-9
the tetra is the chemical the carbon dioxide is the propellent. if you are looking at the right can (red & black with a black cap) then these will be the ingrediants. heres the addy to a forum that has a pic of the proper can you need to look for, check the 5th post down by Wicked_Rain and click on the image link that says TCE.jpg the picture will open in a new window. NO SUBSTITUTIONS http://161.57.220.62/forum/topic.asp?TOPIC_ID=157
Japan Dryer is used when varnishing or shellacing in humid weather. it is added to the varnish or shellac to speed up the drying process. available at hardware stores in the paint section. NO SUBSTITUTIONS
the mix desired is 10 to 1
example: 100 ml TCE 10 ml JD
you want to cover the powdered pill mass with 10 times the amount of fluid which we will call purple beet juice.
example: 1/2 inch of powdered pill mass in quart jar would need 5 inchs of purple beet juice. in this example it would be about 500 ml of purple beet juice needed.
so spray into a clean empty jar 500 ml of the TCE then pour in 50 ml of JD shake well and then pour it on the pill mass in the other jar. let it soak for 3 minutes NO MORE THAN 3 MINUTES. got it? good.
here is the step by step SWIM did in his first test run complete with list of active ingrediants and inactives.
ACTIVE INGREDIANTS
Ephedrine HCL .60 mg
tripolidine 2.5 mg
INACTIVE INGREDIANTS
methylcellulose
lactose
magnesium stearate
polyethylene glycol
silica gel
starch
stearic acid
titanium dioxide
1...ground up pills with mortar and pestle to a fine powder. weight of pill mass was 21.4 grams
2...passed thru a fine sieve used in canning jellies (its all plastic and works great)
3...measured out 100 ml TCE and 10 ml japan drier. mixed together and poured onto pill powder in 1 quart jar. stirred well and let set three minutes.
4...poured entire jar contents thru a funnel with a single filter and no plug. pill mass was an ugly sorta pale blue/grey. sprayed sides of filter down with TCE from the spray can with tube attached. when all pill mass was in bottom of filter it was removed twisted and rung out.
5...opened filter and spread pill mass out on glass plate. as it dried the small clumps were chopped smaller with razor blade. it was left to set untill it was totally bone dry.
6...the dried pill mass was passed thru the fine sieve again. weight of pill mass now 21.2 (a side note of caution here, to avoid the wrath of the wife buy your own fine sieve strainer from canning section of store. dont use hers as it will smell of japan drier untill the end of the time)
7...placed pill mass in clean quart jar. poured in 250 ml of denatured alcohol. stirred let set an hour. decanted, evapped,
repeated two more times.
8...took scrapings from 3 evaps (they were ugly blue/grey (but SWIM had faith in ware and was not worried) ran them through the fine sieve strainer again, poured 100 ml of acetone on the crystals and stirred and stirred and voila white crystals crashing out of tone and the tone was now the ugly blue/grey color. decanted tone spread crystals out on plate to finish drying and they were beautiful snow white crystals SWIM had to put on his sunglasses they were so white lol.
out of a possible 8.6 SWIM`s insane friend got 7.4
now then see, thats a pretty easy technique and it is the latest from the crew at up allnight productions. it kicks everything to the curb including orange gak, orange gakk 2, and povidone, also tryp and chlor. mal. BAM!!! kicked to the curb. i cant stress enough tho so ill say it one more time. FOLLW THE WRITEUP TO THE LETTER!!!!!!!
NO SUBSTITITIONS!!!!!!!! PERIOD!!!!!
when done properly it looks like this pic at another forum. http://161.57.220.62/forum/topic.asp?TOPIC_ID=101
just scroll to the bottom of the opening post and click on the image link. it will open in a new window. thats the way clean E is supposed to look like boys and girls.
class dismissed!
[This message has been edited by Wicked_Rain (edited 12-24-2003).]
[This message has been edited by Wicked_Rain (edited 12-24-2003).]
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#21
 2003-12-24, 23:17
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Infosponge 
Regular
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Re: cleaning psuedo hcl 25mg
lol...here we're about 5 yrs behind you guys...rofl!!!
Until about 8 months ago E had a schedule of about -5 instead of the new 5 rating it has been given...lol
Trust me...there are only binders in our bronco's
[This message has been edited by Infosponge (edited 12-24-2003).]
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#22
 2003-12-28, 08:09
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dan46 
Regular
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Re: cleaning psuedo hcl 25mg
wicked rain
seems a good writeup
i am used to 'seeing videoeditor's writeups
----
for those near mex:
go to pharmacia and ask for ephedra chlordate
pay around 60/oz after haggling--pure
we all know it dissolves in nearly anything<w>
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#23
 2004-01-03, 17:54
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amine_assimilator 
Regular
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Re: cleaning psuedo hcl 25mg
SWIM has had good results using video editors "straight to bee (base)"
is SWIM the only one partial to this technique?
vid claims it to prolly b useful for the forseeable future; true or false? or will only time and adulterants tell?
SWIM is partial to bullseye 60's w/ chlor. mel. $2.50/24
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#24
 2004-01-03, 18:52
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Re: cleaning psuedo hcl 25mg
Well if I were buying pseudo and having to refine them I would recommend buying the 48-60's for $2.98 at Wally World. And use the TCE/JD for a simple and quick start--->to--->finish times. VE's str8t-->2-->E seems like a whole lot of steps and procedures to elicit the same net result as the TCE/JD.
But if this is working for you then Rock-On---->a_a!! <A HREF="http://users.pandora.be/eforum/emoticons4u/smoking/rauch15.gif">http://users.pandora.be/eforum/emoticons4u/smoking/rauch15.gif" width="90" height="90 (http://users.pandora.be/eforum/emoticons4u/smoking/rauch15.gif" width="90" height="90)</A>
Jam.
[This message has been edited by Jamiroquai (edited 01-03-2004).]
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#25
 2004-01-03, 19:05
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kman 
Regular
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Re: cleaning psuedo hcl 25mg
Squirrelgirl, if you aren't going to try a cleaning method EXACTLY the way it's written up, then you must not want to succeed. If I remember correctly, the Str8 to E method calls for boiling your solvents at 105C(for five minutes), not 80C. I suggest that you try the IDEA or Egull method(modified to include japan dryer), depending on whether you're using DMF or NDMF pills.
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#26
 2004-01-03, 19:06
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amine_assimilator 
Regular
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Re: cleaning psuedo hcl 25mg
SWIM hears 'ya Jam, but wally's is kinda far for SWIM to travel, the bullseye dog place is 'round the corner, and the beads are pretty clean.SWIM has yet to find a source for TCE/japan, so, for now it's straight to bee.
BTW, could you post the TCE/japan for SWIM, he misplaced it.
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#27
 2004-01-03, 19:16
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sitbcknchill 
Regular
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Re: cleaning psuedo hcl 25mg
if your talking about the method itself its on the FIRST PAGE...wicked posted it
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#28
 2004-01-03, 19:28
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kman 
Regular
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Re: cleaning psuedo hcl 25mg
Just about any auto parts store will have TCE. She-are-win billies has the japan dryer, or almost any paint store.
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