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Laboratory Tips Safety proceedures, test reagents, drilling rubber stoppers, bending glass tubes, etc. Contributed to by chemists.

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 #1 
Old 2003-12-17, 18:54
FireFly666 FireFly666 is offline
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Default Safrole from Nutmeg

I have read in Total Synthesis 2 by Strike of the www.the-hive.ws (http://www.the-hive.ws) forum that nutmeg contains a good bit of safrole. My question is what are the other impurities? I would like to extract some safrole but I am having trouble finding any reliable info on the procedure. I have done some searches in the following places. www.totse.com (http://www.totse.com) www.the-hive.ws (http://www.the-hive.ws) & www.google.com (http://www.google.com) If I remember right, there was something about the extraction of safrole on the www.chemhead.org (http://www.chemhead.org) website, but the info and other synths have yet to be moved to www.wetdreams.ws (http://www.wetdreams.ws) Thanks for any help!

~FireFly
 #2 
Old 2003-12-17, 23:23
BizzyBee BizzyBee is offline
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Default Re: Safrole from Nutmeg

http://www.ebay.com/ sells sassafras oil 95% safrole content. Craft stores sell it also.
 #3 
Old 2003-12-21, 18:36
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Default Re: Safrole from Nutmeg

Better hurry!!

It's going by way of isofrole.
 #4 
Old 2003-12-21, 20:24
NeverSleepy NeverSleepy is offline
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Default Re: Safrole from Nutmeg

Never heard of isofrole, if you mean isosafrole that is for a different oxidation rather than the simple wacker that most use.

http://www.rhodium.ws/chemistry/wacker.krv.htmlƒ
 
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