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Laboratory Tips Safety proceedures, test reagents, drilling rubber stoppers, bending glass tubes, etc. Contributed to by chemists.

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 #1 
Old 2003-12-16, 01:11
paranoid paranoid is offline
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Default Pure Cafeine

Well, i ' d like to notice that the drug making chemistry bases upon a standard molecule. This is caffeine!

It is widely used as a base in many drugs... Well i'm searching a good and easy way (and somehow cheap!)to purify caffeine extracted from coffe seeds by chloroform. It has to be highly purified!!!

Any ideas?
 #2 
Old 2003-12-16, 01:18
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Default Re: Pure Cafeine

Why not just buy it pure?! http://www.elementalscientific.net/pdf/2003%20Chemicals.pdf

http://www.elementalscientific.net/downloadcat.html

And it is pure.



Enjoy!!

Jam.

[This message has been edited by Jamiroquai (edited 12-16-2003).]
 #3 
Old 2003-12-17, 06:29
eesakiwi eesakiwi is offline
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Default Re: Pure Cafeine

Not a bad idea, a short correspondence course.

Extract caffeine from coffee.

To do it, then describe how it went and the results as well. Acquiring the tools, putting it togeather, getting results.

An accomplishment.

Would help separate the men from the boys?
 #4 
Old 2003-12-17, 23:44
Disaster_Master Disaster_Master is offline
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Default Re: Pure Cafeine

coffee is too complicated. i "made" some pure caffeine over the summer. all it involved was a spoon, a plate, a coffee mug full of hot water, and some coffee filters.

go to dollar tree, buy caffeine pills. crush, dissolve in hot water, filter, boil filtrate down and let remaining water evaporate. very simple, and i got about 10 grams of caffeine for $2.17(stupid fucking 8.25% sales tax).

of course, i'm sure i lost some and it probably wasnt more than 95% pure.
 #5 
Old 2003-12-17, 23:52
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Default Re: Pure Cafeine

The only thing I could think of using pure caffeine for is to cut my heroin.

Jam.
 #6 
Old 2003-12-18, 04:59
ArnoldNailedYourMom ArnoldNailedYourMom is offline
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Default Re: Pure Cafeine

extraction of caffeine from tea (however probably cheaper to buy)

-extract with boiling water first

-rid impurities with calcium salts (calcium carbonate)

-do multiple extractions with dichloromethane

-distill off the solvents (crude product)

-dissolve in acetone by heating

-allow to cool and vacuum filter

should be pretty pure, just check melting point if you have a melt-temp or some sort of apparatus for purity
 
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