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| Laboratory Tips Safety proceedures, test reagents, drilling rubber stoppers, bending glass tubes, etc. Contributed to by chemists. |
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#1
 2003-12-16, 01:11
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paranoid 
Regular
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Pure Cafeine
Well, i ' d like to notice that the drug making chemistry bases upon a standard molecule. This is caffeine!
It is widely used as a base in many drugs... Well i'm searching a good and easy way (and somehow cheap!)to purify caffeine extracted from coffe seeds by chloroform. It has to be highly purified!!!
Any ideas?
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#2
 2003-12-16, 01:18
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Re: Pure Cafeine
Why not just buy it pure?! http://www.elementalscientific.net/pdf/2003%20Chemicals.pdf
http://www.elementalscientific.net/downloadcat.html
And it is pure.
Enjoy!!
Jam.
[This message has been edited by Jamiroquai (edited 12-16-2003).]
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#3
 2003-12-17, 06:29
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eesakiwi 
Regular
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Re: Pure Cafeine
Not a bad idea, a short correspondence course.
Extract caffeine from coffee.
To do it, then describe how it went and the results as well. Acquiring the tools, putting it togeather, getting results.
An accomplishment.
Would help separate the men from the boys?
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#4
 2003-12-17, 23:44
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Disaster_Master 
Regular
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Re: Pure Cafeine
coffee is too complicated. i "made" some pure caffeine over the summer. all it involved was a spoon, a plate, a coffee mug full of hot water, and some coffee filters.
go to dollar tree, buy caffeine pills. crush, dissolve in hot water, filter, boil filtrate down and let remaining water evaporate. very simple, and i got about 10 grams of caffeine for $2.17(stupid fucking 8.25% sales tax).
of course, i'm sure i lost some and it probably wasnt more than 95% pure.
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#5
 2003-12-17, 23:52
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Re: Pure Cafeine
The only thing I could think of using pure caffeine for is to cut my heroin.
Jam.
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#6
 2003-12-18, 04:59
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ArnoldNailedYourMom 
Regular
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Re: Pure Cafeine
extraction of caffeine from tea (however probably cheaper to buy)
-extract with boiling water first
-rid impurities with calcium salts (calcium carbonate)
-do multiple extractions with dichloromethane
-distill off the solvents (crude product)
-dissolve in acetone by heating
-allow to cool and vacuum filter
should be pretty pure, just check melting point if you have a melt-temp or some sort of apparatus for purity
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