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Laboratory Tips Safety proceedures, test reagents, drilling rubber stoppers, bending glass tubes, etc. Contributed to by chemists.

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 #1 
Old 2003-11-19, 21:00
MarkStephan420 MarkStephan420 is offline
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Default Finally!!!

Just wanted to say thank you totse for all your help. My friend said his rxn finally went off. He has one question though. Even though the Eph turned into Meth it was very low quality. What could be the reason for this?
 #2 
Old 2003-11-19, 22:11
jerky jerky is offline
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Default Re: Finally!!!

Maybe Im wrong here, but let me guess "your friends" reaction was actually CASPER THE WIZARDs reaction. Sorry if Im incorrect on this one but it sounds like CASPERS question just posed differently. Maybe Im wrong or just being plain paranoid, wish I could see IP addresses.
 #3 
Old 2003-11-19, 22:17
MarkStephan420 MarkStephan420 is offline
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Default Re: Finally!!!

Im looking for intelligent respones jerk-off. So go fuck yourself and Casper bitch.
 #4 
Old 2003-11-19, 22:27
jerky jerky is offline
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Default Re: Finally!!!

Sorry Guess I was wrong,oops guess I feel like an ass now instead of just paranoid. Nonetheless no need to flame me, I merely expressed a curiosity, wasnting trying to be a jerk-off or give a non-serious answer.
 #5 
Old 2003-11-19, 23:31
RNX57 RNX57 is offline
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Default Re: Finally!!!

how long did the rxn, react. and what sort of stock was used?, hard to say WHY without a bit more input, i;ve dreamt some good n some bad and still find it a puzzel, but dreams are hazy at best, .

RNX57
 #6 
Old 2003-11-19, 23:58
MarkStephan420 MarkStephan420 is offline
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Default Re: Finally!!!

Thank you for your response RNX. He said his reaction went for 3 hours @ 150-170 then 190 for the last 30 minutes. He said he used 1.2-1.4 I2 to E, and 1 to 1 RP to E. Why did it turn out such low quality. Any advise would be helpful.
 #7 
Old 2003-11-20, 00:42
RNX57 RNX57 is offline
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Default Re: Finally!!!

temp n time sound good, tell him to try usen same amounts of E, and IO, swim uses a tad more io than E, swim sticks with a 1/3/3, rp to e to io, and 1/2 the amount of E in distilled, everything dry, sounds like some ido e was left in the final product, unreacted E, not everything was converted. try a 1/3/3 mix, same time and heat...

RNX57

ps: a tad more io and rp is a good idea as this makes the bake....

[This message has been edited by RNX57 (edited 11-20-2003).]
 #8 
Old 2003-11-20, 02:24
kman kman is offline
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Default Re: Finally!!!

Tell your friend to recrystallise next time, and don't be such a smartass punk, or you'll never get any help.
 #9 
Old 2003-11-20, 11:12
jerky jerky is offline
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Default Re: Finally!!!

Just got done screw-in myself as you advised. Anyway so here is my .o2 cents as well, granted Im no chemist or cook. RXN was probably spot on with his diagnosis but also look into quality of precursors maybe. Crap in=crap out like they say. Like RXn said though an abundance of iodine and Rp may help.The extra hydriodic acid would maybe insure complete reaction.
 
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