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Laboratory Tips Safety proceedures, test reagents, drilling rubber stoppers, bending glass tubes, etc. Contributed to by chemists.

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 #1 
Old 2003-11-12, 00:19
greenhorn164 greenhorn164 is offline
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Default a question about iodine extraction?

swim obtained a pint of iodine from the feed store today the bottle says "1 pint equal to 1% titratable iodine.......3.1%v/v" to this swim added 1 pint peroxide, 250 mls water and 25 mls of acid, it has sat for 2 hrs and nothing has developed, untill now swim has been using the 2% tinc and crystals always form after about 30 minutes, swim was wondering if he did something wrong or if this tinc needs more time or what? could someone kindly shed some light? thanks
 #2 
Old 2003-11-12, 03:26
NeverSleepy NeverSleepy is offline
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Default Re: a question about iodine extraction?

you need 7% without the povidone.

the 1% povidone = useless
 #3 
Old 2003-11-12, 03:36
greenhorn164 greenhorn164 is offline
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Default Re: a question about iodine extraction?

sleepy there is no povidone in it only iodine and alchohol?
 #4 
Old 2003-11-12, 03:40
Wicked_Rain Wicked_Rain is offline
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Default Re: a question about iodine extraction?

SWIM thinks you may have added to much peroxide to that mix but not for sure as he has never seen that particular mix.
 
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