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| Laboratory Tips Safety proceedures, test reagents, drilling rubber stoppers, bending glass tubes, etc. Contributed to by chemists. |
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#1
 2003-09-26, 11:48
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lvhustlin 
Regular
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No reaction
A friend of mine got I from tincture using Hydrogen Peroxide and HCL. He got his RP from matches. Cleaned both fairly well but not as much as suggested on totse. he used a 40 40 10 - EIR ratio. When he adds everything in flask he is getting no reaction.. He needs help.
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#2
 2003-09-26, 11:51
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kirby 
Regular
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Re: No reaction
never forgetting that this friend is dreaming
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#3
 2003-09-26, 12:40
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lvhustlin 
Regular
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Re: No reaction
No im serious and he is not dreaming.
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#4
 2003-09-26, 13:02
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kirby 
Regular
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Re: No reaction
no no, you dont understand,,if you tell us its real we cant help you,,,if you tell us the poor blind deaf fucker is dreaming we can add to this dream
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#5
 2003-09-26, 16:05
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gottagogo 
Regular
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Re: No reaction
I don't care what your friend says he's doing. Guys like that lie all the time anyway.
First problem is understanding the rule of clean enough.
Then, you need to look into the mechanism of rp as a reactant, not just a facilitator or recycler of iodine. You need to undrstand the background information as well as the step 1, step 2 info. I'll briefly tell you anyway. You used a .25 ratio of rp, which is probably enough if using a very high quality substance. You are not using a very high quality substance. Even if a seasoned professional, using many secret tricks, cleaned mbrp, the actual content of rp in the resulting fine powder would be considerably lower than 100%. Unused rp is easily recoverable from post rxn mix. Can you see where this is going?
Iodine. Sublime. Easy. Find. Learn. Use more.
No mention of water. I + (D)H2O= HI. Hi there my old buddy. Those two are direct relatives when it comes to watching their their weight. When they get together enough, happy, happy, joy, joy.
Always remember--
Seeing something happening may make you feel all warm inside, but you don't need to see it to know its working. You will find out later (probably much later, but that's ok) that no reaction is the best reaction. (you don't have to get it. Just put it in your pocket for later.)
Don't look so confused. Someone will probably come along and clarify things for your friend. Read the back of a lot more boxes of cracker jacks and you will learn how to use the secret decoder ring that comes inside each specially marked box. If you don't read the label, you'll never know what's inside.
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#6
 2003-09-26, 16:10
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RNX57 
Regular
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Re: No reaction
swim dreams alot, and follows the subcontious ( mm dont look right but dats the teacher) swim fainty seen the ole 1-3-3 mixture. but mr subcontious is leaning twords a 2-3-3 mix in swims next dream, some dreams is a quiet rxn, while another dream was a wild hot puff of yellow?.allthough mr subc does get some goodies (cookies for students) most all the time either way ( he a grade a teacher ole mr subcontious. swim dreams as the above post says.. mr subc cleanes fairly well, and he uses lab grade cry io, match thingies,dh2o.. and semi clean cold remedys..... swim keeps paddling on in dream world. still dreams of pinwheels and such, lot of work though,,, workmanship!
roll alone, less hassels
rnx57
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#7
 2003-09-26, 16:48
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kman 
Regular
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Re: No reaction
Clean your ingredients most diligently! Maybe your friend has money to waste, but swim doesn't.
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