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| Laboratory Tips Safety proceedures, test reagents, drilling rubber stoppers, bending glass tubes, etc. Contributed to by chemists. |
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#1
 2003-09-24, 12:10
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Spook 
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Lend me your brains !!
Hi all
I am trying to put together a modern complete pill to meth synthesis for the laymen (small scale ..NANO ..LOL) using a conglomerate of other peoples methods ..yes i am a laymen myself (i have a good understanding of basic chem but a developing understanding of organic synthesis) and i have to admit this post is completely self motivated..however if i can get it to work i will willingly share all that i have learnt.
I propose to use extracts from the following methods and invite those who are familiar with these methods to answer some simple tech questions ..mainly to do with content and conc of ingredients as i can't find them here and will have to make them myself..and msds's are a bit vague.
1) "the matchbook Red Phosphorus Bible "
(author=unknown )
2) "red phosphorous/iodine meth synth" pfedhcl extraction
(author= Placebo)
3) "nano scale RP/I meth" for actual synth and crystallization..
(author= Curbshot)
I only have a couple of query's, for anyone who is familiar with any of these methods will be able to answer..if you have read this far than it is likely that you may want to help or are at least curious ..all advice/criticism will be gratefully accepted.
If you wish to help answer "shoot"
If you do not wish to help type "boot "
I promise the questions will be concise and direct ..unlike this post ..
thanks in advance .
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#2
 2003-09-24, 12:44
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kirby 
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Re: Lend me your brains !!
lend me your brains,,god that brought back such bad memories,,,my mother use to boil these lamb brains,,then cover them with whipped egg and roll them in bread crumbs,,,then deep fried,,,,jesus that woman made us eat some inhumane food
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#3
 2003-09-24, 14:06
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Spook 
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Re: Lend me your brains !!
Ouch ...yeah that must have hurt ..sorry for the flashback....always dreaded something like that being served up to me and that i was expected to eat it..lol However i must admit i have often wondered what it tasted like ..I.E brains ?? the worst i ever got was liver ..never liked it as a kid and not too long ago i thought "it was just probably just a psycological thing" so i went and ate some ..nup it tastes like shit ..i put it right up there with brussel sprouts !!
experiences are forever ..
Never trust breadcrumbs..
[This message has been edited by Spook (edited 09-24-2003).]
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#4
 2003-09-24, 18:54
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kman 
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Re: Lend me your brains !!
Damn, Kirby, I feel for ya! That shit sounds nasty!
Spook you're proposing to do what swim's been doing, and once swim's satisfied with the yields, swim will put swim's half-assed, slapped-together method.
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#5
 2003-09-24, 23:02
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Spook 
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Re: Lend me your brains !!
Ok no worries..look forward to seeing it ..in the mean time could someone please tell me the concentrations of the H2S04, and hcl "commonly" used in these proceedures what are they ??? I cant make whatever strength i need ..and what the hell is charcoal lighter fluid,,should i be after benzene or is a mineral spirit a suitable replacement??
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#6
 2003-09-25, 18:48
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kman 
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Re: Lend me your brains !!
The HCl swim uses is 31.45%.
Swim's not sure what the percentage of the H2SO4 is(battery acid)but thinks it is 50%.
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#7
 2003-09-25, 19:59
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kirby 
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Re: Lend me your brains !!
charcoal lighter fluid,,same use as zippo lighter fuel i spose,,,they do it to get the ethanol out, i think???,anyway its not a min spirits,,its more a clean light polar that your looking for,,some use hexane etc
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#8
 2003-09-26, 03:29
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Spook 
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Re: Lend me your brains !!
..yeah battery acid can vary...but 50% is good...and i think i can use zippo fluid (butane/propane)but its not the same as charcoal
lighter fluid(benzenz/naptha)..lets hope it does the job.
thank you very much for the assistance..
by the way i am a little concerned about the ratios on the nano method;
1-1.5g E + 3gI + 2gRP = fuck all yeah i know ..
but if the iodine tincture is at 2% active (I2)that is only 0.06g I..?? which is also fuck all..?? 3g of iodine tincture just doesn't seem to be enough or is he somehow extracting the I2 from the tinct first and using that ?? Should i just match the E concentration with neat I2 and go for it ??
[This message has been edited by Spook (edited 09-26-2003).]
[This message has been edited by Spook (edited 09-26-2003).]
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#9
 2003-09-26, 06:24
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kman 
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Re: Lend me your brains !!
You have to get pure I2 out of the tincture. Look for the post titled, "Here it is-all three steps." I forget who posted it, but it's a very informative post.
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#10
 2003-09-26, 08:34
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Spook 
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Re: Lend me your brains !!
yeah i thought as much ..i got pure I2 anyways, thats much easier ..gee im glad i asked that..i will check out the post as well for later reference ..
You all have been a wealth of info ..
Ta.
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#11
 2003-09-26, 14:59
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stillbill 
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Re: Lend me your brains !!
Kirby, you were kidding about the lamb brains?
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