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| Laboratory Tips Safety proceedures, test reagents, drilling rubber stoppers, bending glass tubes, etc. Contributed to by chemists. |
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#1
 2003-09-17, 23:49
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WannaBeChemHead2 
Regular
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Hey Poopeen
Hey Poopeen,
You wanted to be famous.
There is a synth for cat over at the hive. There is no np used and he uses, well, a ton of water (150 for the cleaned pseudo and 265 for the KmnO4(15ml saturated solution + 250 ml dilutant) YOU on the other hand use VERY little water in your a/b. His is really comprehensive and lists all the temperature downfalls, he also uses isopropol alcohol to stop the KMnO4 reaction. Something about almond smell and all that.
My question is - have you ever had a bad batch using the method you listed here? I prefer the a/b reaction to all that water trying to dry out. Can you use pseudo still in its water phase? Meaning that you have de-gaked it but it is still in the water? OR would it be better to a/b the pseudo, dry it and then a/b the cat?
Wannabe
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#2
 2003-09-19, 21:39
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Re: Hey Poopeen
I didnt understand all of your question, so ill say this.......ummm.....ah yes, i have indeed had a BAd batch when i was trying different amounts of pott. perm. It over oxidised, i assume, when i used too much. I have tried it without an a/b after oxidizing, it was not at all good as with an a/b. OOOOoooohhh! I might get it now, do you mean ...nevermind.
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