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Laboratory Tips Safety proceedures, test reagents, drilling rubber stoppers, bending glass tubes, etc. Contributed to by chemists.

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 #1 
Old 2003-09-17, 22:30
Billy_smack Billy_smack is offline
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Default is my method correct?

I'm new to this so let me see. I start with amm nitrate 2 pitchers 4 bottles of lye small amount of water very small. I add fert and lye in cleaned and dry 5 gallon air tank quickly attach nipple valve spout. shake the shit out of it. blow the valve out and connect hose. hose runs 150 ft. coiled in a smallice chest full of liquid propane. amm is cooled and drips into thermos bottle. Never was told measurements so I fill 2 qt. pitcher slightly over 1 inch and add whatever i got out of 6 boxes 48 x 60mg pseudo then drop 3 strips lith and stir and gag till its dry. Also found that it helps to wipe ice from outside of container. Then I pour 3/4 of a jar of colemans on bones stir and let sit while I wash up and catch my breath. Then I filter 4 times through 4 filters (16 filters in all). Next I get a 20 oz. bottle and attach hose to the top pour un iodized salt and add sulfuric acid. then I stick hose in fuel and squeeze very slowly making sure that I don't suck anything up in my hose do this till I get tired and filter repeat from colman step till I get no more reaction. I usually 8-9 gms dried. it burns clean and people like it I just want to make it more crystaline. Have I missed something in my blind bumbling?
 #2 
Old 2003-09-18, 00:25
Atome Atome is offline
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Default Re: is my method correct?

If your NH3 is to manufacture correctly and in good quantity your process must function indeed

Normally one would have to be added can water to stop the effect of NH3 and to pay caution by pouring water bus if lithuim is not entirely to consume by NH3 is the Booooouuummm (it's the risk!!!)

Good luck.
 #3 
Old 2003-09-18, 00:52
Billy_smack Billy_smack is offline
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Default Re: is my method correct?

I'm not totally sure what was just said but the only time I use water is in the amm creation. should I be adding water somewhere else? the closest h2o comes to my lith is in humidity. I threw a strip into a pond to see affect. hmmm dangerous. but what about stopping reaction?
 #4 
Old 2003-09-18, 05:08
kman kman is offline
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Default Re: is my method correct?

you might want to keep a bucket of water around in case something goes wrong, and the annie sucks the water out of your eyes, nose, and flash freezes your skin!
 #5 
Old 2003-09-18, 09:28
kirby kirby is offline
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Default Re: is my method correct?

ok,, it was a bit difficult to diseminate exactly what your saying so no more smoking 6 pipes before posting,,,,,,theory states that only enough ammonia is needed to disolve the sodium metal/lithium,,but,,this has never sat well with me even though i believe it,,,,,,,friends use about 700ml of ammonia for a 2 oz cook, increase on ratio ie 3oz cook needs 1050ml-----now then---add sodium metal to ammonia and allow 3 mins to disolve,,then add psuedo(i use hexane in the A/B and then squirt the hexane and psuedo into the ammonia/sodium metal)(this means you only have to filter the hexane then gas it)(dont add any other solvent after ammonia evaps, its not needed) and stir for 20mins---then add 100ml of water for every oz---allow ammonia to evaporate--now just filter through ONE filter--then gas the hexane and youll see the meth precipitate out--to further purify---read up on crystalization
 #6 
Old 2003-09-18, 22:23
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Default Re: is my method correct?

quote:Originally posted by Billy_smack:

Never was told measurements whatever i got out of 6 boxes 48 x 60mg pseudo then drop 3 strips lith Then I filter 4 times through 4 filters (16 filters in all). Next I get a 20 oz. bottle and attach hose to the top pour un iodized salt and add sulfuric acid. then I stick hose in fuel and squeeze very slowly making sure that I don't suck anything up in my hose do this till I get tired and filter repeat from colman step till I get no more reaction. I usually 8-9 gms dried. it burns clean and people like it I just want to make it more crystaline. Have I missed something in my blind bumbling?



Bro. Next round try 2 strips instead of 3 first of all.

Secondly, do not listen to tales of hexane/toulene/and so on.....

But drop the Colemans man. It has a rust inhibitor in it and it is toxic to the liver.

Also, lessen your non-polar volume to equal close to the volume of alcohol whichever alcohol you used to reduce your filter-fucking-with and to display before youreyes how little of NP is needed! In theory your shit should turn into cottage cheese----meaning that:your volume of liquid NP is replaced by the volume and mass of your dope.



Water is a total tale man!! I challenge anybody to testify using it on a "blowout" episode!! That's just tweeker talk.

You need to weigh your pseudo-extracts'-mass man. For too much Li=vaporized dope rising to the sky! as well as a dirty dope.

And finally 1 liter for 3 ozs. is a total waste of precious annie!!

Remember this:

200ml for first oz.

34ml for each addidtional. Period!

So....that means on a ten gram cook for instance use 7.14ml per gramor rounding up; 72ml for ten grams.

And use this scale(7.14ml per gram)for your ratios up to an oz.

You will see bountiful fruits of your labor spare waated ammonia.

And remember:7grams of pseudo=1 strip of Li.

Only use what you need and buy more pseudo to make more dope with less rounds of cooking since annie is what you got and a 4 pack of batteries=1 oz.

More is less here!
 
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