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| Laboratory Tips Safety proceedures, test reagents, drilling rubber stoppers, bending glass tubes, etc. Contributed to by chemists. |
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# 1

2003-09-12, 01:17
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Regular
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Huntington Beach, CA
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what, if anything, would result from taking iod crystals, rp, psuedo e,dh2o, and just put it all in jar? How long for any would be results?
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# 2

2003-09-12, 03:09
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Try it and see, genius. Heat usually helps.
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# 3

2003-09-12, 03:22
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HMMMMMM.......maybe.......meth!!!!!!!!! Clean your precursors........and try to grab (by reading) some concepts of how/why your reaction will work....then you'll probably understand ratios for different reaction methods. dedicate your time and patience and we'll notice if you really are trying....and we'll help ya.
DD
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# 4

2003-09-12, 03:58
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Seriously dude, there's a viable push-pull method out there, and the nano synth works, too! Fuck! I can hardly type!
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# 5

2003-09-12, 05:18
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Actually, as long as the ratios of reactants were precise in relation to environmental conditions, a room temperature reduction is quite possible and has been successfully done.
It is not recommended though. The whole precise ratios and environmental conditions probably doesn't sound like much, but the guy who says he has done this (and his reputation is such that he has great credibility with me) also has vast experience conducting the rp/i, both short and long. Mostly short. A legend actually.
It takes a good deal of experience not only in the reaction, but the full gamut of reaction conditions that are unique to each individuals habitat.
Search around for room temp rxn.
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# 6

2003-09-12, 05:53
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Regular
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Huntington Beach, CA
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I have been reading all of your guys post's, for a while now and told my friend Rummy. Rummy said he cleaned everything as instructed. RP from cut out striking pads-in atone-siphon-dry, pseudo by denatured Alc.(although it took a few times to figure out that the gatorade bottle he used as a container wasn't thoroughly cleaned out good enough-therefore his psuedo was an orange syrup even though there was no coating on the pill), Iodine, perfect instructions produced perfect results. Distilled water, I loaned him $1.39.
So Rummy throws it all in jar, with ratios in the same proximity as the various instructions seen here. Now he waits, but wonders. Mostly about if and when that violent reaction may occur. Once again, there is no heat. But still he wonders. If nothing by tomorrow, he says he's going to set jar in a water-filled crock pot and set it on low. Would this be wise of him?
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# 7

2003-09-12, 07:00
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No, the crockpot with water is not a good idea. You're boil the water and it'll all just end up evaporating. Plus I think that if you use peanut oil (cause it smokes less than regular) you'd be better off. The act of water boiling might tip your flask or steam would burn your hands. I don't really know....but Switrd would not use water.
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# 8

2003-09-12, 08:02
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Regular
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Huntington Beach, CA
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I will pass it on to Rummy,"no water". Any other suggestion's besides peanut oil? He of course is full aware of the danger's and therefore is looking for the safest ways possible. Time is "not" of the essence in this matter.
He'd also like to know more about the violent reaction/"big dance", like how long this reaction will last, and what should he expect?
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# 9

2003-09-12, 09:26
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I cannot, for the life of me, figure out what compels a person to read for 10 minutes (at best) and then rush out, spend money, go home and procede to "attempt" to perform tasks that involve potentially dangerous chemicals and dangerous legal situations as if they had a full and complete grasp on the entire concept.
I don't mean to slap you around too much, but lets take a look at what you have done:
"Rummy said he cleaned everything as instructed. RP from cut out striking pads-in atone-siphon-dry"
No, must have been the wrong instructions. It would be a not so small miracle if one or two acetone rinses could clean up rp from matchbook strikers. I hate those damn things. Swigotta has reached a point where I write in using gallon sized jugs for the water washes. The method has become quite involved, but its clean in the end. He never knew it was so dark.
" pseudo by denatured Alc.(although it took a few times to figure out that the gatorade bottle he used as a container wasn't thoroughly cleaned out good enough-therefore his psuedo was an orange syrup even though there was no coating on the pill)"
I think that was a bottle of fruit punch gatorade. Chances are the orange color in the gatorade bottle came from those nice pretty white 60's your friend probably used. The kiss of death is using denat alcohol in a straight extraction. I can't think of anything less than 12 years old that water or alcohol can successfully pull with todays pill formulations. It's orange gaak. You pulled pseudo alright. The only problem is you pulled all sorts of shit with it.
"Iodine, perfect instructions produced perfect results."
Lets assume that this is true. The loss will be the greatest tragedy of the story.
It appears that MAYBE there is a bunch of glue and dye from the matchbooks as well as 50-70% of the pseudo weight as gaak. So, he chunked it all in a jar and assumed that's what you do? I guess he didn't get around to reading the reaction part of the process. Not to worry, it is grossly overrated. I am very curious as to how much water he chunked in that jar.
At this point, the best recommendation I could possibly come up with is to first, filter out the red p. I guess the best way to get the pseudo back out would be to A/B it. I sure wouldn't attempt to do that anytime soon. Read it, learn it, then try it. If you completely fuck it up. Do it again on the same stuff. You can't hurt it, right? Who knows, several things could happen. You could accidentally do something right and have a nice thick layer of freebase pseudo come out, the result being you are still clueless as to how it happened, but you still have the pseudo back, and cleaner now too. You may also stumble onto something that pulls the ole lightbulb chain in your brain and you are able to add something you KNOW to your plan.
OK, OK, anyway, the iodine can be recovered last and there is something about that under post reaction iodine recovery somewhere.
If someone knows a better (easier) way to get the pseudo back out, maybe they can share it with you. Other than that, start studying.
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# 10

2003-09-12, 09:58
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Regular
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Huntington Beach, CA
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The RP, Rummy got it off the strike pads completely in one wash. No joke. I think I might know why too. He bought the "Ralphs" brand, and for some reason or another, after he cut the strike pads off he was easily able to get his fingernail under the strikepad and peel it off the paper/matchbook or at least split the paper/matchbook it was glued to. So when he put all the rp strips in the atone, he only had strip the rp from at the worst a paper/matchbook with only half the thickness.
In fact he told me that he put one strike pad in the atone that he didn't split, and that one wasn't even close to come off when all the other one's had been seperated-rp at the bottom and paper/matchbooks floatin' on the top.
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#11
 2003-09-12, 10:23
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kman 
Regular
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Re: iod+rp+e+dh2o=?
Getting the RP off is just the first step. Read the post titled "Here it is-all three steps!" Swik has dreamed about the RIP numerous times, with yields from a few mLs to a nice pile last time(nano method), and swik has learned the difference between so-so, and really clean.
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#12
 2003-09-13, 00:43
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nazelnut-p2p 
Regular
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Re: iod+rp+e+dh2o=?
Check this out,get ride of that shit before you get cracked and go down the street and cop u a sack! It's a lot easier,safer,and cheaper for ya! If you don't have a experienced cook right there with ya helping you threw your just spinning your wheels and wasteing money and time. And you'll end up holding onto all the bad fucked up batches thinkning you can fix them or someone can fix them for you and word will get around cause your asking for help and the next thing ya know your house gets raided and now your going down for 25 years. For manufacturing! That doesn't sound pretty but that will be your reality if you insist on pursueing to be a cook! Leave it up to the big boys who have the years and the pocket. Don't mean to sound like a dick but I've seen it happen way too many times to wanna-bes.
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#13
 2003-09-13, 01:33
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oops_i_od'd 
Regular
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Re: iod+rp+e+dh2o=?
Yeah whatever guy, if my "big boy" would remove his head from his ass once in a while, maybe. But that seems to be impossible for him and that's ok, because my man rummy is work'n on it.
Speaking of Rummy, he's got that mix in the jar sit'n on 150 F. It's got some black/purple smoke, but that's it. There are no layers etc. any suggestion's for Rummy?
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#14
 2003-09-13, 02:48
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gottagogo 
Regular
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Re: iod+rp+e+dh2o=?
Purple smoke? That's the way you know that the reduction is complete. When you see the purple smoke it means that you probably won't even have to bother with an A/B, the shit will precipitate in the solution. All you have to do is filter it off
You may have to wash it a little with acetone, but other than that it will be some killer meth. As good as it gets.
Congratulations. All that time I thought you were just cooking a jar full of shit.
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#15
 2003-09-13, 04:38
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oops_i_od'd 
Regular
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Re: iod+rp+e+dh2o=?
Rummy asks about it being "in solution" and wants to know how to get it out of solution? Precipitating off? like keep letting it smoke off-or precipitate off into a second container. Because yes, there is no doubt that the smoke is purple-but he doesn't see anything solid? just a dark purple solution.
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#16
 2003-09-13, 09:30
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gottagogo 
Regular
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Re: iod+rp+e+dh2o=?
I really should apologize for fucking with you like that. It becomes quite frustrating when you take the time to really think about the situation someone has gotten themselves into, try to figure out what they could do to rectify the situation, and later see that they didn't even read what you had to say. This mostly comes from not getting the answer they were looking for.
So, what I did was give you the answer you wanted to hear just to see if you would respond. Unfortunately, you did exactly as expected.
Sorry to lead you astray. Does anyone have a magical cure for this dude?
As far as this goes:
"got that mix in the jar sit'n on 150 F. It's got some black/purple smoke, but that's it. There are no layers etc. any suggestion's for Rummy?"
The purple smoke is the iodine subliming out of the jar. If you are in mom's kitchen, there is a good chance she is going to kick your ass when she sees that you turned the walls and ceiling yellow. Use bleach to get it off.
Oh, yeah. Remember where this thread is, because when you are through cooking that jar of shit and want to try and salvage as much as you can, I don't want to see the post where you ask what to do with it.
You can't just throw a bunch of shit together and expect it to do what you tell it to do.
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#17
 2003-09-13, 10:51
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oops_i_od'd 
Regular
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Re: iod+rp+e+dh2o=?
Whatever, have your fun. But, don't worry about rum's kitchen, had it covered. He also doesn't undo things- what fails is trash, and he will start from scratch again.
Someone posted an article of the three main ingredient's: rp-iodine-psuedo.
Now, unfortunitely 99% of the synth. out there nobody wants to explain it the simplest way, because they think they're telling 6 yr.olds. Because before the 3-ingredient post, I thought meth was made from anything from ether to vinegar.
So finally after reading nothing but junk, I finally found what I was looking for, "the bottom line". So I told rem to first make sure you have all three ingredient's, in there pure state. Not a bunch of match books, not tincture, and not a bunch of cold pills. So he started with the E and failed three times. Then did something different and that enabled success. 1 down. RP was easy for him-first try success. 2 down. After a hard time finding any tincture with more than 2% he found some with 5% and used the 3 pint peroxide/2 ounce Murietic Acid/1/2 cup dh2o/1 pint of 7% tincture method. Only thing he did different was the tinc was 5%, not 7%. Result's were what looked like a sludge made super small crystals. It did not dry out as expected.
But if he has those three ingredients in their own state. How far off is he?
...and by the way, some of you jackass` ought try and grasp the theory of evolution and the benefits it can produce. It's the only way to find the easiest and best method of all. As more people experiment, the synthesis`will get better and better. Which you yourself will gladly use.
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#18
 2003-09-13, 13:45
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gottagogo 
Regular
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Re: iod+rp+e+dh2o=?
Alright dude, have it all your way. I am here to help those who have really put forth the effort necessary to do a good job. Those like dd and masa are a couple who come to mind. They both listen to those who sincerely try to help like the one you mention, wicked. He has good intentions when he posts writeups like the all in one.
You are a classic example of why it's not always a good idea to lay things out too simplified. There's always someone who just wants to skip the details of why and get to the how. That is exactly what happened to you. You did a halfassed job of cleaning up the precursors (don't come back with, "they were clean". It's obvious that they were not) and then, who knows why, you decided to throw them all together and put some heat under them. You call us jackass? What made you think that's what you were supposed to do?
You've read nothing and know nothing. Take some sound advice even if you already think I'm a dick (and you would have to by now.)
Read enough to at least understand the basic principle behind what you are attempting to do. Doing something without a clue as to why you are doing it is stupid and will result in failure after failure.
And anyone who doesn't want to take the time to "undo" his mistake in an effort to salvage and conserve precious resources has a lot more to learn than the rp/i.
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