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Laboratory Tips Safety proceedures, test reagents, drilling rubber stoppers, bending glass tubes, etc. Contributed to by chemists.

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 #1 
Old 2003-09-01, 23:53
Atome Atome is offline
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Default Reflux time

Hi,

I use 1g Eph, 1.5g I2, 0.6g RP

and also some water drop !

the reflux for a small quantity must it last 36 hours or one can reflux in much less time ???
 #2 
Old 2003-09-02, 06:50
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California
Default Re: Reflux time

This is a much debated topic here. Some will swear by the long slow...and others would bet their lives on a short hot cook. If you would read some other threads, there are probably a dozen or more that were done not too long ago. If you're new to it all, longer is better so there is no question that your shit is completely done. Some guys know when it's done by what it looks like, what it's doing, what the smells are. They've obviously more experience than Switrd. Gotta's done a mess of threads in regard to your question. But like I said

....SEARCH A LITTLE!

[This message has been edited by LwaysTired (edited 09-02-2003).]
 #3 
Old 2003-09-02, 09:15
Atome Atome is offline
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Default Re: Reflux time

Thank you for your reply !!!!!!!
 
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