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| Laboratory Tips Safety proceedures, test reagents, drilling rubber stoppers, bending glass tubes, etc. Contributed to by chemists. |
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#1
 2003-08-20, 21:37
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GoodGuy 
Regular
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Gassing
Hey All.
got a question about gassing when this came up in my last process it got me quite confused so im going to wait until i get an answer.
You need to pipe HCl gas into your jar full of toluene and pseudo freebase, but the gas and your toluene must be dry/no water, or everytime the gas forms crystals it will be reabsorbed by the miniscule amounts of water!
but the gas and your toluene must be dry/no water? is this already achived by srying my tolene before use? and for the gassing process in the other container can i use water with the tinfoil/lye? will that matter as it is just gas going thru and not water?
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#2
 2003-08-21, 03:40
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kirby 
Regular
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Re: Gassing
ok lets start at the beginning,,,why are you gassing the psuedo????
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#3
 2003-08-21, 03:58
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GoodGuy 
Regular
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Re: Gassing
for the powdering process
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#4
 2003-08-21, 04:21
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kirby 
Regular
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Re: Gassing
no, you do that after the reduction,,,,the toluene and psuedo go straightinto the ammonia for reduction
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