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| Laboratory Tips Safety proceedures, test reagents, drilling rubber stoppers, bending glass tubes, etc. Contributed to by chemists. |
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#1
 2003-08-11, 22:04
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em de em aye 
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Could I set up a vacumm distilation using this
Apparatus includes a round bottom borosilicate boiling 500mL flask with 19/38 interchangable joint, Graham type condenser with 200mm jacket and 19/38 joint at the top and an interchangeable stopper. All glassware is borosilicate (heat-resistant). All the junctions are ground glass to ensure a tight seal. This auction comes with a cast iron support stand with a 6" x 9" base and 24" rod, with one single clamp and one adjustable length three finger clamp and a water aspirator.
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#2
 2003-08-11, 22:31
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kronikus 
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Re: Could I set up a vacumm distilation using this
Lab Tips.
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#3
 2003-08-11, 22:33
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em de em aye 
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Re: Could I set up a vacumm distilation using this
Man noone fucken replies in labtits
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#4
 2003-08-11, 22:34
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kirby 
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Re: Could I set up a vacumm distilation using this
are you asking or selling
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#5
 2003-08-11, 22:39
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em de em aye 
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Re: Could I set up a vacumm distilation using this
Im asking fucka but Id sell it for 200
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#6
 2003-08-11, 22:43
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kirby 
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Re: Could I set up a vacumm distilation using this
fucka--who the hell do you think you are--if thats your attitude then no wonder no one answers you---you spoke in your post about an auction---thats why i asked if you were selling---now stick it up your arse for all i care, FUCKA
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#7
 2003-08-11, 22:47
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em de em aye 
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Re: Could I set up a vacumm distilation using this
fukaaaaaaaa isn't an attitude fukaaa
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#8
 2003-08-11, 22:54
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kirby 
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Re: Could I set up a vacumm distilation using this
eat shit and die you cocksucker--you wanna come in here and ask questions then do it civilly--get back to jerk town where you belong and dont forget to bash that condenser up your arse as you go
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#9
 2003-08-11, 23:05
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em de em aye 
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Re: Could I set up a vacumm distilation using this
Go suck a dick you fucken tool, your names god damn "kirby" do you understand how fucking stupid that is.It's pink marshmellow from faggot town.Why don't you head back down to faggot town and continue to get anal pentrated by you animay faggot cartoons you fucken nigger bat
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#10
 2003-08-11, 23:14
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kirby 
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Re: Could I set up a vacumm distilation using this
hahahahaha--i see your going to be real popular in here
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#11
 2003-08-12, 00:04
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em de em aye 
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Re: Could I set up a vacumm distilation using this
It's not a popularity contest you stupid fucken semite
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#12
 2003-08-12, 00:10
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kirby 
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Re: Could I set up a vacumm distilation using this
true--its not--but i happen to be one of the polite cooks in here who answer questions---quite a few others would express there thoughts in a much more vociferous way than i--as im sure you will see after only a short period---so good luck and keep up the good attitude, your persona will bring many a hearty reply
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#13
 2003-08-12, 00:19
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em de em aye 
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Re: Could I set up a vacumm distilation using this
I was asking my friend on this bored his name was fuka thats why I typed fuka at first you flaming marshmellow
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#14
 2003-08-12, 00:24
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kirby 
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Re: Could I set up a vacumm distilation using this
of course you were--how silly of me not to see that--your literacy leaves no room for doubt in what you post---by the way its spelt board---and the only fuka you know is your right hand--try not sexually assaulting it to much
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#15
 2003-08-12, 00:47
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kirby 
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Re: Could I set up a vacumm distilation using this
has it crossed that tiny little retarded mind of yours that you dont have anything to supply a vacumn???? of course it has, your just testing us arent you,,,hahahaha
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#16
 2003-08-12, 01:28
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tryptamine 
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Re: Could I set up a vacumm distilation using this
I could answer your question but unfortunately (for you) it is much better to just say that if you don't know what a pile of glass can do then you will surely be wasting your time buying it.
This thread is a millimol away from being sent to dev/null, tread carefully ya little shithead!
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#17
 2003-08-12, 02:04
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em de em aye 
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Re: Could I set up a vacumm distilation using this
Omg I Im noob just answer why is everyone here such a dickhead
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#18
 2003-08-12, 02:12
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em de em aye 
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Re: Could I set up a vacumm distilation using this
I thought that the water aspirator would be enough to create a vaccum I was wondering
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#19
 2003-08-12, 04:11
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kirby 
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Re: Could I set up a vacumm distilation using this
i firmly believe that the way your being treated has a lot to do with your attiude---and surely your not asking me a question--i know you arent asking tryp cause his opinion of you as an ignorant cunt is the usual factual but short statement he always posts ----perhaps you should ask one of your many friends here in lab tips---or even better---apologize to all here for your attitude and im sure that your questions will be reconsidered and answered--untilyou do--forget it bye
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#20
 2003-08-12, 05:31
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Re: Could I set up a vacumm distilation using this
I
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#21
 2003-08-12, 06:13
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em de em aye 
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Re: Could I set up a vacumm distilation using this
I SINCERLY APPOLOGIZE IF I OFFENDED YOU I KNOW YOU ARE FAR MORE KNOWLEDGABLE THEN I AM CAN YOU PLEASE HELP ME
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#22
 2003-08-12, 06:27
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kirby 
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Re: Could I set up a vacumm distilation using this
thank you--------the set up you describe is good for distilling---i can not see how the water aspirator can supply a vaccum--please explain it to me and why you think it could---the need for a vacumn is to reduce the heating temp required as liquids boil in lower temps under vacumn--or you wish to remove one substance in the liquid ie:safrole oil can be removed by vacumn distillation by setting it at the right temp---ie:you have a mix of methanol and toluene--you wish to take the methanol out so set the temp at 68c--which means only the methanol will evaporate out as toluene evaporates at 110c----in a roto evaporator they have a computer readout where you can set flask rotation speed--flask temp--water temp--vacumn pressure--in the set up you explain your going to require a vacumn display--as a basic you can buy a vacumn gun you can attach--as you pump the handle a vacumn is created and the pressure is displayed on the little guage on the gun--im battling to visualize the aspirator so may be way off her--please explain it --but no matter what--you must get some readouts to be proficient on the unit to be fully operational
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#23
 2003-08-12, 07:51
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Str8_Shooter! 
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Re: Could I set up a vacumm distilation using this
Hey! Did'nt know ya' posted here(lol!)...Hows ya' mutha'fuka?
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#24
 2003-08-12, 08:09
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kirby 
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Re: Could I set up a vacumm distilation using this
if thats to me str8 im doing fine
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#25
 2003-08-12, 18:54
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FireBomb 
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Re: Could I set up a vacumm distilation using this
hey tryptamine or one of the other mods could you lock/delete this as it is a waste of time and bandwith on our TOTSE server thanks a lot
Ohhh on a second note: em de em aye You are one stupid mother fucking idiot if you would have been polite ranther than getting you pantys in a wad then your question would have been answered. Ohhh and your lucky we dont have stricter rules here at TOTSE because if there were and I was an ADMIN your ass would be baned mother fucker.
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#26
 2003-08-12, 19:15
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em de em aye 
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Re: Could I set up a vacumm distilation using this
thanks for that flamefire or whatever.Anyways how could I set up a vacuum.I thought the water aspirator could like pump the air out or soemthing.I dunno what should I use to make a vacuum
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#27
 2003-08-13, 01:02
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tryptamine 
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Re: Could I set up a vacumm distilation using this
MDMA thank you for the apology.
This setup will work for vac distillation, however the aspirator will work for most vac needs but it won't build up enough vacuum to distill your ketone. You need a mechanical pump of some sort.
Another note, while using a graham condenser in a distillation setup you must setup for downwards distillation otherwise the condenser will block itself and cause sputtering and backing up, if not something worse.
A side note(yes I 'm bragging)I'm getting a second vacuum pump for free, barely been used and it pulls a vacuum down to a few mm's.
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#28
 2003-08-13, 10:21
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malware 
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Re: Could I set up a vacumm distilation using this
quote:Originally posted by kirby:
has it crossed that tiny little retarded mind of yours that you dont have anything to supply a vacumn???? of course it has, your just testing us arent you,,,hahahaha
You guys need to max and relax, the guy didn't say "fuka" in a hostile way...you dirty chemists need to stop cooking so much cat and crank.
[This message has been edited by malware (edited 08-13-2003).]
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#29
 2003-08-13, 10:31
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Str8_Shooter! 
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Re: Could I set up a vacumm distilation using this
Kirby, It wasn't to you man, it was to em de em aye or whatever's boy Fuka! But I'm glad do here you're doing good!
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#30
 2003-08-13, 15:33
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Str8_Shooter! 
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Re: Could I set up a vacumm distilation using this
[QUOTE]Originally posted by malware:
[B] You guys need to max and relax, the guy didn't say "fuka" in a hostile way...you dirty chemists need to stop cooking so much cat and crank.
If that's the way you feel why the fuck are you here? And if you had a lick of sense, or read the whole thread, it'd be clear the guy was rude, runnin' his dick-sucker, just like you........And I do mean that in a hostile way...FUKA.
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#31
 2003-08-13, 15:38
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kirby 
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Re: Could I set up a vacumm distilation using this
way tp go str8,,give em some texan attitude mate
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