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Laboratory Tips Safety proceedures, test reagents, drilling rubber stoppers, bending glass tubes, etc. Contributed to by chemists.

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 #1 
Old 2003-08-11, 22:04
em de em aye em de em aye is offline
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Default Could I set up a vacumm distilation using this

Apparatus includes a round bottom borosilicate boiling 500mL flask with 19/38 interchangable joint, Graham type condenser with 200mm jacket and 19/38 joint at the top and an interchangeable stopper. All glassware is borosilicate (heat-resistant). All the junctions are ground glass to ensure a tight seal. This auction comes with a cast iron support stand with a 6" x 9" base and 24" rod, with one single clamp and one adjustable length three finger clamp and a water aspirator.
 #2 
Old 2003-08-11, 22:31
kronikus kronikus is offline
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Default Re: Could I set up a vacumm distilation using this

Lab Tips.
 #3 
Old 2003-08-11, 22:33
em de em aye em de em aye is offline
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Default Re: Could I set up a vacumm distilation using this

Man noone fucken replies in labtits
 #4 
Old 2003-08-11, 22:34
kirby kirby is offline
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Default Re: Could I set up a vacumm distilation using this

are you asking or selling
 #5 
Old 2003-08-11, 22:39
em de em aye em de em aye is offline
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Default Re: Could I set up a vacumm distilation using this

Im asking fucka but Id sell it for 200
 #6 
Old 2003-08-11, 22:43
kirby kirby is offline
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Default Re: Could I set up a vacumm distilation using this

fucka--who the hell do you think you are--if thats your attitude then no wonder no one answers you---you spoke in your post about an auction---thats why i asked if you were selling---now stick it up your arse for all i care, FUCKA
 #7 
Old 2003-08-11, 22:47
em de em aye em de em aye is offline
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Default Re: Could I set up a vacumm distilation using this

fukaaaaaaaa isn't an attitude fukaaa
 #8 
Old 2003-08-11, 22:54
kirby kirby is offline
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Default Re: Could I set up a vacumm distilation using this

eat shit and die you cocksucker--you wanna come in here and ask questions then do it civilly--get back to jerk town where you belong and dont forget to bash that condenser up your arse as you go
 #9 
Old 2003-08-11, 23:05
em de em aye em de em aye is offline
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Default Re: Could I set up a vacumm distilation using this

Go suck a dick you fucken tool, your names god damn "kirby" do you understand how fucking stupid that is.It's pink marshmellow from faggot town.Why don't you head back down to faggot town and continue to get anal pentrated by you animay faggot cartoons you fucken nigger bat
 #10 
Old 2003-08-11, 23:14
kirby kirby is offline
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Default Re: Could I set up a vacumm distilation using this

hahahahaha--i see your going to be real popular in here
 #11 
Old 2003-08-12, 00:04
em de em aye em de em aye is offline
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Default Re: Could I set up a vacumm distilation using this

It's not a popularity contest you stupid fucken semite
 #12 
Old 2003-08-12, 00:10
kirby kirby is offline
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Default Re: Could I set up a vacumm distilation using this

true--its not--but i happen to be one of the polite cooks in here who answer questions---quite a few others would express there thoughts in a much more vociferous way than i--as im sure you will see after only a short period---so good luck and keep up the good attitude, your persona will bring many a hearty reply
 #13 
Old 2003-08-12, 00:19
em de em aye em de em aye is offline
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Default Re: Could I set up a vacumm distilation using this

I was asking my friend on this bored his name was fuka thats why I typed fuka at first you flaming marshmellow
 #14 
Old 2003-08-12, 00:24
kirby kirby is offline
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Default Re: Could I set up a vacumm distilation using this

of course you were--how silly of me not to see that--your literacy leaves no room for doubt in what you post---by the way its spelt board---and the only fuka you know is your right hand--try not sexually assaulting it to much
 #15 
Old 2003-08-12, 00:47
kirby kirby is offline
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Default Re: Could I set up a vacumm distilation using this

has it crossed that tiny little retarded mind of yours that you dont have anything to supply a vacumn???? of course it has, your just testing us arent you,,,hahahaha
 #16 
Old 2003-08-12, 01:28
tryptamine tryptamine is offline
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Default Re: Could I set up a vacumm distilation using this

I could answer your question but unfortunately (for you) it is much better to just say that if you don't know what a pile of glass can do then you will surely be wasting your time buying it.

This thread is a millimol away from being sent to dev/null, tread carefully ya little shithead!
 #17 
Old 2003-08-12, 02:04
em de em aye em de em aye is offline
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Default Re: Could I set up a vacumm distilation using this

Omg I Im noob just answer why is everyone here such a dickhead
 #18 
Old 2003-08-12, 02:12
em de em aye em de em aye is offline
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Default Re: Could I set up a vacumm distilation using this

I thought that the water aspirator would be enough to create a vaccum I was wondering
 #19 
Old 2003-08-12, 04:11
kirby kirby is offline
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Default Re: Could I set up a vacumm distilation using this

i firmly believe that the way your being treated has a lot to do with your attiude---and surely your not asking me a question--i know you arent asking tryp cause his opinion of you as an ignorant cunt is the usual factual but short statement he always posts ----perhaps you should ask one of your many friends here in lab tips---or even better---apologize to all here for your attitude and im sure that your questions will be reconsidered and answered--untilyou do--forget it bye
 #20 
Old 2003-08-12, 05:31
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Default Re: Could I set up a vacumm distilation using this

I
 #21 
Old 2003-08-12, 06:13
em de em aye em de em aye is offline
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Default Re: Could I set up a vacumm distilation using this

I SINCERLY APPOLOGIZE IF I OFFENDED YOU I KNOW YOU ARE FAR MORE KNOWLEDGABLE THEN I AM CAN YOU PLEASE HELP ME
 #22 
Old 2003-08-12, 06:27
kirby kirby is offline
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Default Re: Could I set up a vacumm distilation using this

thank you--------the set up you describe is good for distilling---i can not see how the water aspirator can supply a vaccum--please explain it to me and why you think it could---the need for a vacumn is to reduce the heating temp required as liquids boil in lower temps under vacumn--or you wish to remove one substance in the liquid ie:safrole oil can be removed by vacumn distillation by setting it at the right temp---ie:you have a mix of methanol and toluene--you wish to take the methanol out so set the temp at 68c--which means only the methanol will evaporate out as toluene evaporates at 110c----in a roto evaporator they have a computer readout where you can set flask rotation speed--flask temp--water temp--vacumn pressure--in the set up you explain your going to require a vacumn display--as a basic you can buy a vacumn gun you can attach--as you pump the handle a vacumn is created and the pressure is displayed on the little guage on the gun--im battling to visualize the aspirator so may be way off her--please explain it --but no matter what--you must get some readouts to be proficient on the unit to be fully operational
 #23 
Old 2003-08-12, 07:51
Str8_Shooter! Str8_Shooter! is offline
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Default Re: Could I set up a vacumm distilation using this

Hey! Did'nt know ya' posted here(lol!)...Hows ya' mutha'fuka?
 #24 
Old 2003-08-12, 08:09
kirby kirby is offline
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Default Re: Could I set up a vacumm distilation using this

if thats to me str8 im doing fine
 #25 
Old 2003-08-12, 18:54
FireBomb FireBomb is offline
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Default Re: Could I set up a vacumm distilation using this

hey tryptamine or one of the other mods could you lock/delete this as it is a waste of time and bandwith on our TOTSE server thanks a lot

Ohhh on a second note: em de em aye You are one stupid mother fucking idiot if you would have been polite ranther than getting you pantys in a wad then your question would have been answered. Ohhh and your lucky we dont have stricter rules here at TOTSE because if there were and I was an ADMIN your ass would be baned mother fucker.
 #26 
Old 2003-08-12, 19:15
em de em aye em de em aye is offline
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Default Re: Could I set up a vacumm distilation using this

thanks for that flamefire or whatever.Anyways how could I set up a vacuum.I thought the water aspirator could like pump the air out or soemthing.I dunno what should I use to make a vacuum
 #27 
Old 2003-08-13, 01:02
tryptamine tryptamine is offline
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Default Re: Could I set up a vacumm distilation using this

MDMA thank you for the apology.

This setup will work for vac distillation, however the aspirator will work for most vac needs but it won't build up enough vacuum to distill your ketone. You need a mechanical pump of some sort.

Another note, while using a graham condenser in a distillation setup you must setup for downwards distillation otherwise the condenser will block itself and cause sputtering and backing up, if not something worse.

A side note(yes I 'm bragging)I'm getting a second vacuum pump for free, barely been used and it pulls a vacuum down to a few mm's.
 #28 
Old 2003-08-13, 10:21
malware malware is offline
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Default Re: Could I set up a vacumm distilation using this

quote:Originally posted by kirby:

has it crossed that tiny little retarded mind of yours that you dont have anything to supply a vacumn???? of course it has, your just testing us arent you,,,hahahaha

You guys need to max and relax, the guy didn't say "fuka" in a hostile way...you dirty chemists need to stop cooking so much cat and crank.

[This message has been edited by malware (edited 08-13-2003).]
 #29 
Old 2003-08-13, 10:31
Str8_Shooter! Str8_Shooter! is offline
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Default Re: Could I set up a vacumm distilation using this

Kirby, It wasn't to you man, it was to em de em aye or whatever's boy Fuka! But I'm glad do here you're doing good!
 #30 
Old 2003-08-13, 15:33
Str8_Shooter! Str8_Shooter! is offline
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Default Re: Could I set up a vacumm distilation using this

[QUOTE]Originally posted by malware:

[B] You guys need to max and relax, the guy didn't say "fuka" in a hostile way...you dirty chemists need to stop cooking so much cat and crank.

If that's the way you feel why the fuck are you here? And if you had a lick of sense, or read the whole thread, it'd be clear the guy was rude, runnin' his dick-sucker, just like you........And I do mean that in a hostile way...FUKA.
 #31 
Old 2003-08-13, 15:38
kirby kirby is offline
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Default Re: Could I set up a vacumm distilation using this

way tp go str8,,give em some texan attitude mate
 
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