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Laboratory Tips Safety proceedures, test reagents, drilling rubber stoppers, bending glass tubes, etc. Contributed to by chemists.

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 #1 
Old 2003-07-31, 17:59
Atome Atome is offline
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Default Rhoduim Process Red P/Iodine Reduction

What is used the assembly as bottle on last the photograph?

http://www.rhodium.ws/clandestine/nano/index.html http://www.rhodium.ws/clandestine/nano/nano9.jpg

The rp/i mixture and water are mix with toluenes?

which are these gases thus it speaks ?

Thank you for help !
 #2 
Old 2003-07-31, 22:44
morgan morgan is offline
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Default Re: Rhoduim Process Red P/Iodine Reduction

hello my little curry munching friend--good to see some life out of india--im not getting a good picture down here and it is difficult to see--im only guessing here and hope others have a better input---looks like a bottle with hose attached to end--id say he is mixing salt and sulphuric acid in the bottle to produce the gas needed to solidify the meth oil in solution---i use two glass jars--one has sulphuric acid99% in it (150ml)--the other has hydrocloric acid34% as a hypochlorite solution(50ml)--the two glass jars are connected by a 6mm tube--from the bottom of the sulphuric jar to the top of the hydrocloric jar--a tube also is inserted into the lid of the sulphuric jar--and a hose leads from the hydrocloric jar which is used to convey the gas to the solution requiring gassing---i have the sulphuric jar on a step making it higher than the hydrocloric jar---i now blow on the hose leading to the sulphuric jar--this starts the acid to drip down into the hydrocloric jar--as it drips slowly it begins to produce the required gas--which forces its way out the hose from the hydrocloric jar and into the solution requiring gassing---one tip---take hose out of solution requiring gassing--as when the acid stops dripping suck back occurs which will suck all your product into the hydrocloric jar as such ruining it--good luck and dont forget you live in a country where they hang your arse if caught
 #3 
Old 2003-08-01, 00:18
Atome Atome is offline
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Default Re: Rhoduim Process Red P/Iodine Reduction

For you this bottle contains the mixture rp/i ready for the gaz hcl ?!?
 #4 
Old 2003-08-01, 00:54
morgan morgan is offline
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Default Re: Rhoduim Process Red P/Iodine Reduction

hi atome--im sorry friends only do the birch using ammonia and sodium metal--not what you are doing which is the red phos iodine reduction--none the less--when yourve cooked the red phos iodine ephedrine mix and allowed to cool--you must filter off all remaining red phos( this red phos can be cleaned and used again)--this should leave you with the now fully cooked meth in a solvent solution--this should appear a clear solvent with a syrupy like opaque substance fully disolved into the solvent--it is now this solvent with with said syrup in it that is gassed with hcl--gas for 20 secs then filter--keep gassing and filtering(never gas for longer than 20 secs before filtering out white precipitace)until no more white precipitace comes out of the solvent--good luck
 #5 
Old 2003-08-01, 01:01
morgan morgan is offline
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Default Re: Rhoduim Process Red P/Iodine Reduction

went off on completely the wrong track there--sorry--no this bottle appears to hold the rock salt- sulphuric acid which is combined to make the gas used to gas the solvent as i described in the previous message---in my first message to you, i described the method my friends use to create the same gas--or you can go the way displayed in the picture--which is place approx 100 grams of rock salt in a bottle, add 100ml of sulphuric acid, attach hose to bottle top making sure it has a airtight seal--as the gas is created it is forced out of this hose and you direct this flow through the solvent requiring gassing
 #6 
Old 2003-08-01, 01:07
morgan morgan is offline
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Default Re: Rhoduim Process Red P/Iodine Reduction

when you put the ephedrine into the redphos-iodine mix to be reduced--the ephedrine should be in toluene--from what ive read it is about 6mls of toluene for every 1 gram of ephedrine to be reduced
 
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