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Laboratory Tips Safety proceedures, test reagents, drilling rubber stoppers, bending glass tubes, etc. Contributed to by chemists.

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 #1 
Old 2003-07-21, 19:07
loutre bottom mistress loutre bottom mistress is offline
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Default still have a few questions

Ok first of all swil will try and explian what going on: swirl extracted psuedo by means of soaking crushed pills in d-alky for about an hour durning this time swil shakes then filter liquid through 3 coffee filters(it took forever) then repeat filtering three more time or untill liquid was clear then microwave untill almost dry then blow dry with hairdryer then add small amount of dh20 just enough to dilute pm then put in freezer of 30min or so untill the solution is kinda icey then filter 3 more time micowave and blow dry the psuedo smell kinda like end products that swil has smelled from swim before.

rxn time: add 3gm of p 2gm of lbrp and 3.5gm of lbi2(3,2,3.5) then add 1.5-2.5ml of dh20 cover with balloon and let reflux at 140F for 24hrs then checked and turned up heat to 175F for 24hrs when checked again the rxn smelt like pusedo.then rxn was liquid and never went dry but it was a bright red color that you could see through. WHAT HAPPEND?

ok other dreams that swil has had was the same on pill extracting and same run set up but only cooked for 7hrs at 140F then 160F for another 8hrs or so and but the liquid was clear and smelt of dog shit kinda not cat piss then after post reaction results were lye tasting crystals(powder)or so swil thought but after trying another way to extract pill from yellow(h**t)let crushed pills soak for 30mins then filter through 5 coffee filters 3 times then microwave and blow dry when swil boiled down it didn't smell like anything or aleast all the other psuedo swil had done so swil thought its already fucked up so swil added hot iso-alky and almost desolved the pm then let sit forever and nothing so put in freezer and still nothing then put in microwave and boiled down opened the door and it was still lots of liquid so swil got busy and let it alone with the microwave door open when swil returned the liquid was gone and powder stuff in the middle of the bowl and pinwheel crystals on the outter edges and around the powder so swil scraped up the crystals only and rinsed with acetone then let dry when swil tasted the stuff it bit swils tongue like the end product before. so now swil scraped up middle and tasted its kinda bitter(not as bad as the crystals) and kinda taste like meds. should swil combine the stuff and try an a/b or throw it out?

also the yeild was very poor like started with 3-4 gms and ended with 1.5-2gms.

p.s swil knows to try the STE next time but is trying to find gooood chems.
 #2 
Old 2003-07-22, 00:09
cranknymph cranknymph is offline
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Default Re: still have a few questions

hey miss...this is how swinc does the pills. so far so good... crush as fine as possible. add 3x denatured alcohol to mass, shake for 1 min, let settle for 1/2 hr, use turkey baster (glass), carefully extract liquid only. if any pm in liquid, let sit for 1/2 hr, re-extract. using same baster, stuff 10 cotton balls in narrow neck and pack tight. wet with clean denatured alcohol before filtering. after cotton balls are wet down with denatured, filter extracted solution through the cotton balls. take filtered fluid, carefully pour onto large mirror or glass, let air dry, don't rush. you will see contaminents, also a lot of pinwheels. process not finished yet! after completely drying, scrape mass off of glass. put pm in glass container. use generous amount of mek. swirl for about 15 secs let sit for 5 min. psudeo will not dissolve in mek, but contaminents will. simply pour off mek, let psuedo air dry until you no longer smell mek. now you are ready to re-disolve in denatured alcohol just enough to dissolve mass and then a pinch. pour out on mirror and let air dry. watch some of the prettiest pinwheels form!!
 #3 
Old 2003-07-22, 02:10
pikk pikk is offline
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Default Re: still have a few questions

well this wont work on the pills where swip lives . but here is a tip for you two when you add the denat(swip says use meoh it is a lot better about pulling and wont burn your sudo as easy) to your pill mass stir it up really well now let it sit for about 20 min then stick it into the freezer for about a hour . it will clear up the acohol alot faster and the pill mass at the bottom will get kind of hard so you can pour out the luqid alot easier.
 #4 
Old 2003-07-22, 04:05
morgan morgan is offline
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Default Re: still have a few questions

try washing the pill mass before extracting your eph--you will have a much better result--check out the methods at rhodium--
 
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