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| Laboratory Tips Safety proceedures, test reagents, drilling rubber stoppers, bending glass tubes, etc. Contributed to by chemists. |
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#1
 2003-07-10, 07:08
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KraKleBack KinG 
Regular
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report on VE's Straight to E
someone is curently doing VE's straight to E extraction with only 10,000 mg of 30mg psuedo's.
11:40pm: began mixing solvents
11:45 had to the store real quick
1230am returned... siphoned off dry layer
added pills
1245 placed on mid-hot hotplate
now he is typing this waiting for it to boil..
update shortly.
could methyl alc be added if you feel there was not enough IPA?
[This message has been edited by KraKleBack KinG (edited 07-10-2003).]
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#2
 2003-07-10, 07:50
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tReePHrOg 
Regular
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Re: report on VE's Straight to E
yeh methanol would actually be better to
use on any Dry matrix formation pills,
regardless of solvent dryness, methanal is just theat much closer to acetone than isopropyl. also when doing your reflux
fuck the sand trap, fire up your backyard
propane gas barbecue stand and cook me a hot dog while your not busy losing all your hair.
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#3
 2003-07-10, 08:26
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KraKleBack KinG 
Regular
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Re: report on VE's Straight to E
could someone mix the methly and ipa?
busy with other shit but
200 am filtered off first pull... easy so far
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#4
 2003-07-10, 08:38
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tReePHrOg 
Regular
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Re: report on VE's Straight to E
yeh mix 1/2 and 1/2 but still keeping
enough heat (boiling) to actually see bubbles
coming to surface. I think iso-propyl evaporates slightly slower than methanol so
when you start to lose alcoholic volume
always add more methanol, psudoo will dissolve in both iso-and methanol.
probably better in methanol than iso- but not by much.
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#5
 2003-07-10, 08:43
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KraKleBack KinG 
Regular
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Re: report on VE's Straight to E
thanks
i knew that but i just wanted to make sure since they said follow directions exactly
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#6
 2003-07-10, 09:19
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KraKleBack KinG 
Regular
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Re: report on VE's Straight to E
about 3AM finishing last pull off pill mass... looks good so far
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#7
 2003-07-10, 10:04
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tReePHrOg 
Regular
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Re: report on VE's Straight to E
on a recent set of posts a smart person said that when evaporating your pulls, bont neccesarily boil but keep it at like 90 celsius? or you will lose pseu to boiling.
if that seems like it might take too long,
a smart person also said they use the microwave to evaporate alcohol from psudu pulls, only thing is if you do decide to microwave a litre or two of this at a time,
heat it but then DONT open the door, Im thinking methanol wont ignite without a flame BUT may ignite if absolutely hot enough
then ventilated with open air, like wait 50 seconds before retiming and starting a 3-5minute heating phase with micro, or fuck what I'm saying and boil the methahol till gone.
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#8
 2003-07-10, 11:20
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KraKleBack KinG 
Regular
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Re: report on VE's Straight to E
fucked up night. i have to go help my boy about to be in some deeep shit. so, i HAVE to wait to boil it.. i was considering using the microwave, thats how we always evap the heet(methyl). but i didnt know about nuking some naptha.
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#9
 2003-07-10, 11:33
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Wicked_Rain 
Regular
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Re: report on VE's Straight to E
phrog...he is doing a therotical new extraction process dumbass the directions dont call for a microwave. if you would bother reading past threads here you might have a fuckin clue as to what you are talking about.
[This message has been edited by Wicked_Rain (edited 07-10-2003).]
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#10
 2003-07-10, 18:45
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tReePHrOg 
Regular
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Re: report on VE's Straight to E
I apologize I don't theoretically use VE's
method although resaerch tells me its best
for any DMFormations and or adulturants.
But if evaporation is neccessary a lower heat evaporation may be neccessary if any waxes,or oxygen binders exist in the final
phase 1 product, therefore not to bake the damn crap together with the psuepoo and it be unrecoverable by seperation by another lesser or more CH consistent solvent.
I apologize that I not stupid though , Ill shutup now.
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