About
Community
Bad Ideas
Drugs
Ego
Erotica
Fringe
Society
Technology
register | bbs | search | rss | faq | about
meet up | add to del.icio.us | digg it
Go Back   Community > Science > Laboratory Tips
Register FAQ Members List Calendar Search Today's Posts Mark Forums Read

Laboratory Tips Safety proceedures, test reagents, drilling rubber stoppers, bending glass tubes, etc. Contributed to by chemists.

Closed Thread
 
Thread Tools Display Modes
  #1   Add Str8_Shooter! to your ignore list  
Old 2003-07-01, 11:41
Str8_Shooter! Str8_Shooter! is offline
 
Dallas, Texas U.S.A.
Default

AM has brought to Swiss' attention that a new "dopefuckerupper" has been added to a good deal of the wht. 60's. This creature of the deep has been destroying Swiss' quality and quanity and perplexing Swiss and makeing him look like a "person who could no longer produce killer chili". I was dumbfounded, embarassed, and angry with myself for a while because this predator was lurking in my chili, and I didn't know it. He according to the man, quietly lurks in the shadows, darkening your rxn fluids, and springin into activity when you attemt to raise the ph. This is no joke, I just wanted to let everyone know.
  #2   Add AlwaysTired to your ignore list  
Old 2003-07-02, 05:55
AlwaysTired AlwaysTired is offline
 
California somewhere....
Default

Well...........what the heck is it?
  #3   Add gottagogo to your ignore list  
Old 2003-07-02, 06:47
gottagogo gottagogo is offline
 
Default

Its called yesterdays news. The orange gaak is nothing new. Most people find it when using methanol or isopropyl to pull the pills. Denatured alcohol is ok and the new one by Video Editor has proven itself with P/8's, L434's, L450's, and 257's. These are for sure. In lower concentrations it may look pink. Xylene crashing after the ve method is complete will keep ya safe and clean.
  #4   Add poopeen to your ignore list  
Old 2003-07-02, 10:50
poopeen poopeen is offline
 
Default

from my book

"Methyl Orange; An organic dye used as an acid-base indicator. It changes from red below pH 3.1 to yellow above pH 4.4 (at 25c) and is used for titrations involving weak bases."

there is also a methyl red that is quite similal except in color.''''shift
  #5   Add Str8_Shooter! to your ignore list  
Old 2003-07-03, 07:49
Str8_Shooter! Str8_Shooter! is offline
 
Dallas, Texas U.S.A.
Default

I had no orange tint at all in my (well filtered) liquid E or in my dry, crystalized E. However, Swiss' final rxn fluid has been dark brown, and he's doing the same process that usually produces Killa', so he doesn't think that its because not all iodine has been burned off, but sadly chili has not been killa.

???Skark? Something else???
  #6   Add gottagogo to your ignore list  
Old 2003-07-03, 11:55
gottagogo gottagogo is offline
 
Default

No, you're right. Your pseudo can be perfectly snow white and powder dry and still have that shit in it. One way to know for sure is when you clean your post rxn RP. After it has been rinsed out good and it is ready to be cleaned up so it can be used again, put some acetone in it and stir it up. Wait a few minutes and see if the liquid turns colors. Anything from light pink to a medium orange is messed up, but you can still pull good shit from it. Just a little less of it. Final xylene crash will take care of it.
  #7   Add Str8_Shooter! to your ignore list  
Old 2003-07-03, 14:05
Str8_Shooter! Str8_Shooter! is offline
 
Dallas, Texas U.S.A.
Default

Thanks Gotta,

So, are you saying this shit doesn't effect potency, only yield?

Also,is this why Swiss' Rxn fluid has been so dark, and has such a "sweet", not so good dopey smell? Or has he, perhaps, gotten off kilter with his crystals? Time/temp? Swiss doesn't think so. When he first started getting dark, sweet smelling rxn fluid, and not such great shit, he thought, "Not cooking iodine out, cook longer". Still the same. "Raise temp a little, cook longer". Still the same. What the fuck? Swiss is perplexed, confused and furious, but most of all embarassed....Swiss is used to making THE killa'for Christ's sake. Gotta? Anybody? Swiss ain't down for sub-par product resulting from his craftsmanship. Please help.
  #8   Add gottagogo to your ignore list  
Old 2003-07-03, 17:44
gottagogo gottagogo is offline
 
Default

When you have recrystallized and rinsed the crystals with acetone, then reduce the volume of the resultant rinse, does the liquid turn a progressively darker brown as it evaporates? When it has evaporated completely is there a brown oily, sweet smelling residue (sometimes with some meth still in it)?

If so, you may be dealing with aunt PEG.

The answer is, of course, xylene.
Closed Thread

Thread Tools
Show Printable Version Show Printable Version
Email this Page Email this Page
Display Modes
Linear Mode Linear Mode
Hybrid Mode Switch to Hybrid Mode
Threaded Mode Switch to Threaded Mode

Posting Rules
You may not post new threads
You may not post replies
You may not post attachments
You may not edit your posts

BB code is On
Smilies are On
[IMG] code is Off
HTML code is Off
Forum Jump

 
To the best of our knowledge, the text on this page may be freely reproduced and distributed.
 

totse.com certificate signatures
 
 
About | Community | Bad Ideas | Drugs | Ego | Erotica | Fringe | Society | Technology
Hot Topics