Ok, i just have a few questions for some you you birchers out there. what would someone use as a rxn vessel. And then, when your reaction is done, and all the Anne has evaped, where does the water come from that is suppose to be in the bottom of the container, if i understood right, then you mix some colemans with the water, seperate, gas the colmans, filter, dry acetone wash, then use a duel solvent if you want for the final step.. does all this sound about right?

Any help would be really apprecated.

oh, and after you have your Anne in a container :not rxn, just storeing container:, little unused propane tank, nitrous tank for car, if you put that in a freezer for awile, and get it real cold, can you just pour it into your reaction vessel, or do you need to do something speacial? thanks in advance.

quote:Originally posted by OZs2KEYs:

Ok, i just have a few questions for some you you birchers out there. what would someone use as a rxn vessel. And then, when your reaction is done, and all the Anne has evaped, where does the water come from that is suppose to be in the bottom of the container, if i understood right, then you mix some colemans with the water, seperate, gas the colmans, filter, dry acetone wash, then use a duel solvent if you want for the final step.. does all this sound about right?

Any help would be really apprecated.

oh, and after you have your Anne in a container :not rxn, just storeing container:, little unused propane tank, nitrous tank for car, if you put that in a freezer for awile, and get it real cold, can you just pour it into your reaction vessel, or do you need to do something speacial? thanks in advance.

as for a rxn vessal swim likes jars . just pick the size that fits your rxn.

there does not need to bee any water .

yes if you get it real cold it is easier to deal with but a reguler freezer wont get it cold enough for it to be all lquid . so turn your bottle on its side to get the lquid out not the gass. or you could get a lab annie bottle thay pull of the bottem .