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Laboratory Tips Safety proceedures, test reagents, drilling rubber stoppers, bending glass tubes, etc. Contributed to by chemists.

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  #1   Add Masahed to your ignore list  
Old 2003-06-28, 17:52
Masahed Masahed is offline
 
UK
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If so could you do a cut & paste for SwiM?

Thanks.
  #2   Add lukkydleprachan to your ignore list  
Old 2003-06-28, 19:24
lukkydleprachan lukkydleprachan is offline
 
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I just did a cut and paste for that over in another thread. It's the newest method, using less peroxide by Geezmeister.

Lukky D
  #3   Add Masahed to your ignore list  
Old 2003-06-28, 23:23
Masahed Masahed is offline
 
UK
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Ta SwiL. I'll go find it.
  #4   Add RiffRaff to your ignore list  
Old 2003-06-28, 23:39
RiffRaff RiffRaff is offline
 
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YEs,

I am very interested in what technique

is being used to make iodine using peroxide

in the mix.

now i'm not asking the recipe but just the name of the technique. if you could pass that on i would appreciate it Lukky

. and I know you most likly hate me and thats cool to.It whats makes the world turn.

Right on

Rif
  #5   Add cranknymph to your ignore list  
Old 2003-06-29, 00:18
cranknymph cranknymph is offline
 
lost
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anyone know when this site will be back up or any other info on it? i have been directed there for my research, but have not been able to get to the site
  #6   Add lukkydleprachan to your ignore list  
Old 2003-06-29, 10:55
lukkydleprachan lukkydleprachan is offline
 
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Give it some time. CH will be back. It's just making some major changes.

Things should be back online soon, but some "kinks" are currently being worked out.

Keep the Faith.

Lukky D

WWW.chemhead.ORG
  #7   Add arfer d. barfer to your ignore list  
Old 2003-06-29, 11:49
arfer d. barfer arfer d. barfer is offline
 
Sans Merde Parish, LA USA
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Yes, I have a copy. No, I will not cut & post.
  #8   Add Masahed to your ignore list  
Old 2003-06-29, 12:04
Masahed Masahed is offline
 
UK
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Quote:
quote:Originally posted by arfer d. barfer:

Yes, I have a copy. No, I will not cut & post.
Ooooh! Fucking idiot. Why bother posting?

Anyone other than this dickhead:

SwiM has solved his problem with I2, but he's dying to check the yield. How long must it be left wrapped over epsoms before it can be checked? Is 24hrs enough?

  #9   Add cranknymph to your ignore list  
Old 2003-06-29, 18:59
cranknymph cranknymph is offline
 
lost
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thanks for info. i keep checking for the site, so will just keep checking. any info that could be cut and pasted here would be greatly appreciated. i am looking for anything w/iodine crystallization techniques for my paper and am at a stand still.
  #10   Add cranknymph to your ignore list  
Old 2003-06-29, 20:40
cranknymph cranknymph is offline
 
lost
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one additional question. what is the purpose for the idoidine?
 #11 
Old 2003-06-30, 04:08
gottagogo gottagogo is offline
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Default Re: Has anyone got a copy of the "Making Iodine" CH archive?

This motherfuckin totse. I just posted a reply that took me a fuckin hour. when I got up off the bed, I hit a key or something OBVIOUSLY WRONG, and the son of a bitch went to another page. When I returned, you guessed it, gone. Every god damn unsaved word.

Sorry masahed, I'll try again later.
 #12 
Old 2003-06-30, 04:23
Masahed Masahed is offline
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Default Re: Has anyone got a copy of the "Making Iodine" CH archive?

Thanks dude, much appreiciated. SwiM say's he managed to muddle his way through. Although it would still be nice to see the original.

At any rate, seems some other dudes want a peek.

WHERE HAVE YOU GONE CH? WHAT DID WE DO?? haha.
 #13 
Old 2003-07-02, 11:31
RiffRaff RiffRaff is offline
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Default Re: Has anyone got a copy of the "Making Iodine" CH archive?

cranknymph

one additional question. what is the purpose for the idoidine?

Well Crank. The Iodine starts the reactions

with your other reagents."the cooking"

I hope that helps you

Riff
 #14 
Old 2003-07-03, 23:24
gottagogo gottagogo is offline
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Default Re: Has anyone got a copy of the "Making Iodine" CH archive?

First, let me say

riff--iodine is the most important part of the reduction reaction. It and water form hydiodic acid which reduces pseudo to meth.

masa--sorry about screwing up your name. I didn't even realize there was another name so close to yours until you pointed it out. I'll go back and change it now. Didn't want to until I made this post.

Gott with swigotta about the iodine from 2% tincture and he said to tell you the super simplified, just a few words version. I thought he was joking and tried to explain that gotta doesn't do anything with just a few words and he gave me a piece of paper with it already written down. Of course, if I wrote what he did it would look like this:

I did this. Do the same-

1.5 L tinc.2%-- jug 1 gal.-- hcl 34% 750 ml. --stir-- wait 20 min.-- H2O2 1.4 L. add 250 ml./min.-- stir cont.-- freezer 2 hrs.-- remove-- filter thru paint strainer 2 layer-- vacuum-- rinse well DH2O-- vacuum dry-- coffee filters 15 roll-- squeeze under foot-- repeat-- break up rock-- weigh-- small jar on cardboard-- cover with jar-- freezer 6 hrs-- remove-- weigh-- clean dry jar inside big jar-- epsom salt-- lid tight-- done.

Not happy with yield 86g. after freezer--before epsom dried (24 hrs)

Sounded ok to me, but he was upset because he had to get some sleep and didn't refilter the leftovers. Probably would have been at least 6-8 more grams.

You know, not only is shit like that impersonal, it looks like jibberish to newbies. Take a look and see what you think. Perhaps a fully notated version will follow. I have to quit making promises as this is taking too many life points. Ya know what I'm sayin'?
 #15 
Old 2003-07-04, 01:50
Masahed Masahed is offline
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Default Re: Has anyone got a copy of the "Making Iodine" CH archive?

Nice one. Ta SwiG.

SwiM says he has 500ml of 2.5% ready to roll but found his first experiment FAR too easy, which suggests something was overlooked!!

Now he has something with a bit more substance to work with, he's back to his happy preoccupied self!

He hopes he didn't come across as petty with the marased thing, normally it wouldn't matter, but if you read the guys posts (when CH returns) you will understand why he wanted to make it clear that it wasn't him.

He already has his own incompetence to deal with, he don't want someone else's! Haha.
 #16 
Old 2003-07-04, 05:28
pikk pikk is offline
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Default Re: Has anyone got a copy of the "Making Iodine" CH archive?

masa bro send me a email adress . and i will give you what geez just sent me yesterday on this subject. ...my email is in my profile

pikk
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