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| Laboratory Tips Safety proceedures, test reagents, drilling rubber stoppers, bending glass tubes, etc. Contributed to by chemists. |
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# 1

2003-06-24, 00:50
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SwiM says his tiny but very focused intellect is now concentrating on the dual solv, with pfed.
The last (first) time he attempted this he got nothing, what did he do wrong? He:
Covered evap (small casserole) dish with boling IPA to supersaturation, added 5* the amount of boiling 'tone, poured into shot glass size jar, made airtight & put in freezer for a few hours.
When he went back there were no crystals crashed into the jar, why could this be?
As always, all info/guidance is much appreiciated.
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# 2

2003-06-24, 02:02
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ok my first question is was your actone dry ? i have to ask
second was this a nano ?( if so dont bother )
5 times the amout of tone seems like alot to me.
but her is how swim does it . take 1 oz of meth put into small pryex dish pour in meoh enough to desolve meth now i evap this till a skin forms across the top . now pour a little meoh into just enough to desolve the skin.
ok now pour in 2 shots(shot glasses) of actone put this in the freezer till you get what you want . now if you want big xtals let it room temp evap .this takes longer so if you need it fast put half in the freezer . you get the idea
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# 3

2003-06-24, 02:21
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The 'tone is dry & the amount is 1g of pfed (don't wanna use more since it's just a practise run), too small to be worthwile? Ta for that.
SwiM should probably go see a doctor, thinks he's got an OCD with pseudo cleaning, haha.
Probably time to be happy with what he's got & just move on to the next step.
Thanks for the info though, no doubt it will prove useful in the long run.
Ta.
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# 4

2003-06-24, 03:38
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OK I admit it. I wasn't paying attention when I first read the post. Its OK though. This will work for either. Just leave out the part about taking out that sample to enjoy while you wait.
Dude, dude, dude!!
Wait a minute. Pikk. Tsk. Tsk.
Masa, my man. When you give praise to the meth gods tomorrow, make sure the props go to the king of dual solvents
Worlock
This first part is from Swigotta's notebook of idiot savant ramblings, deciphered by me, your loyal servant.
If you have a small amount of meth, use an appropriately scaled down jar. Swigotta's favorite, 6 ounce (180 ml) baby food jar. You can do a shitload in that little jar.
First, lets pretend that the shit is still drying on the pie plate. When those dirty little gemstones are dry. (All the way dry is good, but almost all the way dry is ok too)
Now scrape the shit up with a razor blade and scrape it into the baby food jar. Get it all.
Then add just enough denatured alcohol to dissolve it all.
Put the jar on your heat source. Swigotta uses mantles with controllers, so he didn't really notate time, temp, and important shit like that. Anyway, the bottom of the jar gets just hot enough for it to take about 3-4 seconds before you say, "Ahh, damn. That son of a bitch is hot." when you put your hand on the bottom of the jar.
OK, this should go without saying, but .....
WHILE THE JAR IS BEING HEATED, NEVER, EVER, LEAVE IT. NOT EVEN FOR A MINUTE. YOU WILL BURN THE SHIT UP AND WILL WANT TO COMMIT SUICIDE, OR WORSE, MURDER WHEN YOU DO! SAVE A LIFE, PISS YOUR PANTS!
With that said, heat it up for a couple of minutes, then take the jar (not by the bottom. Remember?) and hold it in front of your evaporation system (fan) and swirl it around for about 30 seconds. Do this back and forth until it all crystallizes (this is why you use the least amount of alcohol necessary to dissolve (mostly dissolve. Heat will do the rest) your shit (goodies))
Paranthesis are good.
***Warning*** Technique dependant step
Now set up a filter on another jar and flash the contents of the jar. This means take an eyedropper (the big kind called battery tester at wally's, $0.97) and squirt DRY, AND I MEAN IT BETTER BE FUCKIN' DRY, acetone into the jar and rinse it all into the filter. Squirt a little more DRY, SAHAHA DRY acetone over the sparkling pile of diamonds then let this dry.
SAVE THE REMAINING LIQUID FOR LATER, EVAP AND DO IT AGAIN.
THIS IS CALLED [b]CRYSTALLIZATION[b]
This is the Worlock dual solvent recrystallization technique.
It makes no difference whether its a gram or a kilo. Everything is gauged by your eyes, so I hope ya ain't blind.
Perhaps it can work with other solvents in the same way, but I cannot vouch for them.
Take the crystallized meth that you just made, and after you tap out a bit of a sample for testing purposes (and to compare the before and after quality), put the shit (remember, its still shit) into a baby food jar.
Then add DRY, I'M TELLIN YOU IT BETTER BE SO DRY YOUR SKIN PEELS WHEN IT GETS TOO CLOSE TO IT, acetone until you think its enough. I'm serious. As long as the shit is covered by about an inch, it doesn't matter. Acetone is not the controlling factor in this (or any other dual solvent technique. The controlling factor is always going to be the solvent in which the shit is most soluble.)
Now, put the jar on the heat. Heat it up enough to bubble the acetone.
***Warning*** Technique dependant step
When it begins to bubble, add denatured alcohol (others like isopropyl work, but the crystal formation is different and I cannot vouch for the technique being applicable) a little at a time. For starters, it probably takes about 9-10 mls. per gram. Take it slow, but don't take all day either. What? I said it was technique dependant.
The trick is to add just enough alcohol to ALMOST COMPLETELY DISSOLVE ALL OF THE METH. Did you see the key word there. ALMOST. ALMOST. ALMOST.
You have to get a feel for this one. Here's a little clue. It don't hurt nuthin' if you don't add enough, but it won't do nuthin' if you add too much.
Get it? Gott it! Good.
Now take the metamorphosing (I looked it up) duckling off the heat and gently put it down on a cloth or wooden countertop (it would be a shame to crack the glass on a cold marble countertop) and put the lid on it tight.
Let it sit out for a couple of hours (if you have time) then put it in the freezer for a coupla hours. No matter what, don't put the hot or warm jar in the freezer. Period!
The idea here is to cool the jar as slowly and evenly as possible. The slower it cools, the larger the crystals will be.
When you take them out of the freezer, make sure you have a filter already set up.
Wipe the jar of (carefully, don't disturb the swan inside just yet) any ice and moisture. This is important as water ...well just get it all).
Now, just open it up and rinse with DRY, FUCKIN' DRY MOTHERFUCKIN' acetone. If you chill this acetone first, its even better. Some say its positively necessary.
Rinse them into a filter over a jar and rinse them while in the filter with a coupla squirts more. Let them dry. Then chunk them in the trash cause this beautifully clean swan will bite you!
Don't forget the rinse jar. There are starving meth heads all over the world who would kill for that jar.
I was just wondering.......
Did you get the point about the acetone being dry?
I hope so.
[This message has been edited by gottagogo (edited 06-24-2003).]
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# 5

2003-06-24, 03:53
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Thanks SwiGotta. Much appreiciated.
SwiM says he's sure that his 'tone is dry since a sample of it has been sitting over some rock salt for a few days & has not yet managed to dissolve it. It's the only test he could think of.
He has read the info given but thinks it will take a while to fully digest it. He hopes he can come back & ask about specifics when he does get a grip on it!
Many thanks.
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# 6

2003-06-24, 04:20
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Just read the edit & am probably pissing up the wrong tree, but the sample is sitting in a test tube away from the bottle of stuff to be used. It was just a dryness test.
*thinks the edit was for someone else but thought he would mention it anyway*
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# 7

2003-06-24, 12:18
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masa--
the edit was because I didn't see that you were talking about pseudo instead of meth. The technique works for both, but you can't take out a sample of the pseudo to smoke while you wait. It would be way too gross.
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# 8

2003-06-24, 14:57
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Understood, ta for clearing that up. It was late & SwiM was drunk so his comprehension was a bit shit!
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# 9

2003-07-10, 03:42
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first of all, if i am missing something noted, i searched through threads to try and figure out what swinc did wrong, but not able to come up with anything, so i have to ask! swinc followed dual solvent instructions, but came up with nothing left 2 times. let cool to room temp (put in freezer once, and let cool room temp all the way 2nd) and still nothing. any ideas?
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# 10

2003-07-10, 07:26
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yeh, the best idea is to add some methamphetamine to you "dual" solvents.
see...once the solvents evaporate,
crystal methamphetamine will appear.
Secondly, no offense but gottago sounds like hed be better off masturbating than chatting in these forums. With phrases like,
"dirty little gemstones" ,um ""acetone over the sparkling pile of diamonds then let this dry." and "MOTHERFUCKIN' acetone"MOTHERFUCKIN' acetone" he'd get off
just looking at my hand blown glass dick,
"That I blew! wehoo!That I MUTHERFUCKING blew
all by myself!! yay!" dude stay away from my girl fagget, ITs CALLED GLASS/METHAMPHETAMINE because of its DENSITY
they are not diamonds you silly hoebag.
And last but not very at the least, gottago says, "If you have a small amount of meth, use an appropriately scaled down jar. Swigotta's favorite, 6 ounce (180 ml) baby food jar. You can do a shitload in that little jar. First, lets pretend that the shit is still drying on the pie plate""
Nah,,, fuckhead I thought I'd try and stuff
32 ounces of my good dope into that tiny jar sinci I can fit a shittload in there. Gotta,
dude Ive seen more glass/dope in a fuckin
sandwich bag that would overfill your little
contraption hoebag. Only now I see how absolutely immature you are by this very post
chek it out you old fogey fucker, stay off drugs and take Tylenol PM with your evening water bath , I'm glad I don't know you in person you babylon puff the magic dragon sorcerer hoebag. I starting to think you
really are a fictional character. Flapping your wings around totse trying to breath fire
at my reaction flask and shit.
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#11
 2003-07-10, 08:38
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46method 
Regular
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Re: Dual Solvent recystallisation.
FROG; ur a little prick if swim has ever seen 1. swim has been sitting back learning on this site for awhile before swim ever registered. swim is probaly old enough to have seen the cum stain on the blanket laying on the hood of the car that you were concieved from.
swim is not the chemist type and yea, swim only knows birch. why do u think swim is here(to learn)? but for the past 25 yrs swim has kept swim and a few friends very happy.
you at times seem like a very knowledgable person but u make people not want 2 read ur post with your smart ass mouth. swim is still learning about the birch method every day(as of last night!!!!!!!!!! can u get 110g of kick ass shit from 144g of clean sueie, well swirl (another"old fogey fucker" did) and wants to hear from those that r more knowledgeable in the areas of swims dreams.
u are attempting to sling shit at one the most respected and knowledgeable dreamers on this site, like it will hurt swigotta's rep(ha, ha). so let the magic dragon fly and spread wisdow.
so FROG, slim, slim' sista or whichever the fuck u want 2 be today. LIKE this site and RESPECT those that teach or get the fuck off this site.
damn, did swim just write that! gotta, pikk(4 your help, thanx) and all that r willing to teach truthly because of the love of our dreams keep it up. you know that this will always happen(smartass punks wanting to be the "king pin") so just look past and keep dreaming.(and teaching) damn swim said it was kick ass!!!!!!!!!!
[This message has been edited by 46method (edited 07-10-2003).]
[This message has been edited by 46method (edited 07-10-2003).]
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#12
 2003-07-10, 09:39
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tReePHrOg 
Regular
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Re: Dual Solvent recystallisation.
I apologize, Ibi-polar.
I have a lot of young smartass friends thats were I get that bad attitude.
I apologize for the magic dragon remark.
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#13
 2003-07-10, 11:55
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gottagogo 
Regular
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Re: Dual Solvent recystallisation.
Aaahhh! That's the beauty of cyberspace. You have time to think before you act.
You see froggy, Swigotta has an ill temper, the likes of which I hope you have never had the displeasure of experiencing. It can be quite embarrassing to be with him when someone, not unlike yourself, gets cocky and begins to mouthe off. Fortunately for you, this is not reality. The playing field is leveled when it comes to physical attributes which leaves Swigotta at a disadvantage.
BUT.....
I'm not Swigotta and I know that the advantage goes to the one who is most aptly qualified to respond to slanderous, immature posts.
So, I would like to address the areas where you have obviously misunderstood my writing styles as well as touch on a few oversights regarding my educational background (without, of course, going into any detail).
nymph--
Along the way, I would like to try to help you understand this technique as it is indespensible if your goal is quality.
Frog--
Right off the bat you said:
"see...once the solvents evaporate,
crystal methamphetamine will appear"
This is absolutely wrong. The concept of ANY dual solvent recrystallization revolves around the solubility of the substance you want to crystallize in the two(hence the word dual) solvents chosen.
In other words, an ideal dual solvent would be one solvent that the product is very soluble in when hot and insoluble in when cold and the other would be the opposite. (I don't think there is one of these, but it's just an illustration to make a point.)
And the point is--
You do not evaporate to obtain the crystals. They grow out of the solution as the solution cools. Since acetone has the ability to supercool, it becomes a good choice for the freezer technique. First year college chemistry.
Now, this next part is purely personal, so if you are looking in this post for assistance with the D/S, skip ahead.
Froggy, when I read the part about poppin my pud, floggin the dolphin, spankin the monkey, chokin the chicken.........sorry, I got a little carried away there.....anyway, it was funny as hell. At first I couldn't even tell that you were trying to insult me. It really sounded like wit. You know what wit is, don't ya? Well, I hope so, 'cause it is the basis of my writing style. If you are not aware of the definition of the word "wit", please go and look it up in Webster's. Go ahead, I'll wait.
Hum dee dum dum dee.................Hmmmm.....yep, there's still a little left in here..........I wish the wife would hurry back. I hate to load this thing myself.
OK, you're back. Now that you understand how the posts are worded, I would like to share that your analysis really made me think (That's what intellectuals do. Look it up later, we don't have time right now.) I started thinking about why I use so much sexual inuendo in my writing. I don't have an answer yet, but I really never thought about it before. I think I'll talk to the wife about that. (That's what intellectuals do also) Your attempt to relate caused me to ponder your gender. I assumed from the beginning that you are male, but if you have a hand blown glass dick and you are male, heterosexual, I would have to ask "why?"
OK, that's enough of the personal stuff. Now, back to the subject at hand.
Dual solvents are for growing crystals "in solution".
Here's some more slight inaccuracies:
froggy writes:
"ITs CALLED GLASS/METHAMPHETAMINE because of its DENSITY
they are not diamonds"
The street term "glass" originated when aminorex hit the scene and became popular. Meth cooks started using it because buyers were asking for glass thinking it was better than meth. It is better than crank. It is not better than meth. Oh, and it's not called glass meth because of it's density either. It looks loke aminorex because of it's crystal purity which makes it long, thick, and clear. When you wash a pile of crystals that have been dual solvented with cold, dry acetone, and you have cool white lighting, they look EXACTLY like a pile of sparkling diamonds. Or, so I've heard.
Now, when I stated that you can put a "shitload" of meth in a baby food jar, I was speaking relatively. You understand what I mean by relatively speaking don't ya? No, it doesn't have anything to do with your uncle Willie. It's kinda like some guy in Kentucky with a half dozen of those 22L rb flasks readin' your post and sayin', "Damn boy, 32 ounces, when you gonna gett serious and start makin' sumpin' that will last mor'n one day."
I was speaking to someone who had already stated that he was using very small quantities and experimenting, trying to expand his knowledge base and perfect a new technique. It is important to listen to those whom you desire to help. Only then will you truly be able to help.
At first, I wanted to be insulted by the following statement:
"Only now I see how absolutely immature you are by this very post"
but I soon realized that those who are quick to judge, quick to anger, and slow to understand are characterized as immature. It seems ironic that you would call me immature in a post where you define yourself as such. You must use caution when posting. Once the submit button is pressed, you cannot change what has been written. Sure, you can go back and edit or delete the post, but not if someone else has already saved it. Which I have done with yours. I also have loddymercy's stuff and suttliar's and many more. I like to save them for posterity. They are quite funny and most memorable to read.
I have wasted entirely too much time responding to this post. I actually did it because someone out there whom I don't even know, stood up for me. I appreciate it and decided that I should explain myself although I knew it probably wouldn't be necessary.
My friends and family say I talk way too much, so I guess it's true.
The bad part is that there is a lot of productive topics to talk about, and now I have wasted all of my time with this bullshit.
nymph--
I'm sorry. My time would have been better spent trying to help figure out what you may be doing wrong. There is a very good chance you are putting in too much alcohol. It's really late and the wife is going to come back in here and ask me why I'm still on the computer, but I owe you at least this:
Put meth that you have scraped up off a dry plate into an appropriately sized jar. Add a quantity of acetone, that has been previously dried over epsom salt, to the jar that is enough to cover the pile of somewhat dirty meth by about an inch. This amount is not important to get accurate. THE ACETONE DOES NOT CONTROL THE RECRYSTALLIZATION. Put the jar on medium heat. Use caution when heating so you do not break the jar. When the acetone begins to bubble a bit, add A FEW DROPS of denatured ethanol and stir. If you are using <1 gram of meth, you must pay close attention to the contents of the jar. There is a fine line between just enough and too much. As the solution gets closer to the boiling point continue adding drops of alcohol AS LONG AS THERE ARE STILL UNDISSOLVED CRYSTALS IN THE BOTTOM OF THE JAR.
YOUR GOAL IS TO HAVE A FEW CRYSTALS STILL IN THE BOTTOM OF THE JAR WHEN IT REACHES A FULL BUT GENTLE BOIL. WHEN IT IS REMOVED FROM THE HEAT, THE LAST OF THE CRYSTALS WILL DISSOLVE AWAY, AND THE CRYSTALLIZING PROCESS WILL BE SET IN MOTION.
Remember to tightly secure the lid immediately upon removal from heat. (Swigotta alwys filters immediately after removal from heat, but don't worry about it right now.)
The basic principle from this point on is too cool the solution as SLOWLY AND EVENLY as possible. If this is not convenient for you, don't worry. As soon as it is cool enough not to crack the glass, pop it in the freezer and leaqve it there for at least 2 hours. Oh, when you get it right, please post whether or not SWIY thinks the pile in the filter looks like diamondsa or not, would ya?
Do you hear what I'm sayin'!?
PS--Again, I did not proofread. Please forgive mistakes.
[This message has been edited by gottagogo (edited 07-10-2003).]
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#14
 2003-07-10, 18:16
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cranknymph 
Regular
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Re: Dual Solvent recystallisation.
hey gotta...thanks for info (nymph and swinc think you rule!!) will let you know!
phrog...why ya dissin people?
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#15
 2003-07-10, 18:31
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tReePHrOg 
Regular
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Re: Dual Solvent recystallisation.
I said I apologize Im bipolr I just
read what I wrote Im so sorry now I just
hate myself. I have only done re-x-izations
with acetones, I never thought about frezzer
growing stuff though. Based on this dual solvent technique I might try the 3/4 acetone
to 1/4 denatured mix, seems like it might
work in th freezer. Ihave only done xtallizations with pebbles/powders with acetone at room temp. nowhere near experienced as Gotta though, hell I didn't know crystals would "grow" from acetone in the frizerator.
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#16
 2003-07-11, 05:35
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gottagogo 
Regular
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Re: Dual Solvent recystallisation.
froggy--
I would think that you're schizophrenic or something. One minute you're spouting off technical shit that I don't even understand, the next you're whining like a little girl (don't take that too harshly).
You are incorrect in your assessment of my experience. Swigotta is coming along, but I am still doing the same thing that I always have--
Reading and writing.
Worlock is where I found this information and Swigotta's notebook is the only way that I know it works.
Please reread the post if you are serious about the technique because according to your post you don't understand the concept yet.
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#17
 2003-08-25, 18:42
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stillbill 
Regular
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Re: Dual Solvent recystallisation.
Damn, is this some good reading or not!!!
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