About
Community
Bad Ideas
Drugs
Ego
Erotica
Fringe
Society
Technology
register | bbs | search | rss | faq | about
meet up | add to del.icio.us | digg it
Go Back   Community > Science > Laboratory Tips
FAQ Members List Calendar Search Today's Posts Mark Forums Read

Laboratory Tips Safety proceedures, test reagents, drilling rubber stoppers, bending glass tubes, etc. Contributed to by chemists.

Reply
 
Thread Tools Display Modes
 #1 
Old 2003-06-17, 20:34
stillbill stillbill is offline
Regular
 
Default Lukky D?

Swis recently found a 50ml. boiling flask and was curious to know would this size

vessel be capable of doing a 2 grm. nano?

As always, thank you!
 #2 
Old 2003-06-18, 08:13
lukkydleprachan lukkydleprachan is offline
Regular
 
Default Re: Lukky D?

It should be fine, as long as the balloon is extra sturdy, or is otherwise taped to a piece of extended tubing or such.

Is the flask tall, or does it have a longer neck? This will be a crucial factor.

Also, super clean RP will help, as then it will occupy less space, as less weight is needed.

Lukky D
 #3 
Old 2003-06-18, 15:01
stillbill stillbill is offline
Regular
 
Default Re: Lukky D?

Lukky D, the flat bottom flask has a neck

that extends 2" above the round part of the flask. Is this adequate? The top of the neck

has a nice flared lip for a balloon to be attached. Swis will make sure about the sturdy balloon and taping it. Extra cleaning of the rp also!
 #4 
Old 2003-06-18, 20:29
lukkydleprachan lukkydleprachan is offline
Regular
 
Default Re: Lukky D?

It sounds fine, but remember that it will be safer to run this reaction with less heat. Keep an eye on it.

Make sure to really powder all precursors with a good mortar and pestle. This will get them all as fine as possible for mixing, and also should take up less space.

Lukky D
 #5 
Old 2003-06-18, 22:46
stillbill stillbill is offline
Regular
 
Default Re: Lukky D?

thanks Lukky D
 #6 
Old 2003-06-18, 23:58
pikk pikk is offline
Regular
 
Default Re: Lukky D?

sb swim has found that using the hose with the ballon at the end of the hose is a lot better . not as much pressure, meaning the ballon wont pop as easy .
 
To the best of our knowledge, the text on this page may be freely reproduced and distributed.
 

totse.com certificate signatures
 
 
About | Community | Bad Ideas | Drugs | Ego | Erotica | Fringe | Society | Technology
Hot Topics