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Laboratory Tips Safety proceedures, test reagents, drilling rubber stoppers, bending glass tubes, etc. Contributed to by chemists.

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 #1 
Old 2003-06-13, 20:17
Oxycodone Oxycodone is offline
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Default Diethelamine

Does anyone have any good ideas on how to add d to my ls without listed precur ie what is the best redily avalible pre for

also morphine into diacetalmorphine without acetic anhydryde

Thanks in advance
 #2 
Old 2003-06-13, 22:47
DrY.R.Head DrY.R.Head is offline
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Default Re: Diethelamine

It could be posible to estrafy it with a combonation of glacial acedic acid and H2SO4 & heat as a catalyst. This hypothetical RXN should be anhydrous too.

The alph-hydroxy group on ephedrines can be estrafied in this way, so I suspect that it should work for morphine too.

[This message has been edited by DrY.R.Head (edited 06-13-2003).]

[This message has been edited by DrY.R.Head (edited 06-13-2003).]
 #3 
Old 2003-06-14, 05:45
Smokey the Bear Smokey the Bear is offline
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Default Re: Diethelamine

quote: Does anyone have any good ideas on how to add d to my ls without listed precur

Synthesize the diethylamine yourself. :rolls eyes:
 #4 
Old 2003-06-14, 23:05
Oxycodone Oxycodone is offline
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Default Re: Diethelamine

Yea dude I understand that I mean from what?
 
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