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Laboratory Tips Safety proceedures, test reagents, drilling rubber stoppers, bending glass tubes, etc. Contributed to by chemists.

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 #1 
Old 2003-06-11, 09:32
DaMethuzereth DaMethuzereth is offline
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Default Providone-Iodine Solution 10% Is this OK for push/pull I2 crystals?

Is Providone-Iodine Solution 10% usable in making Iodine crystals? Would a tinted dish prevent enough light from degrading the I2 Crystals? I read the label, and it goes on to say that this solution is equivilent to 1% Iodine. I guess the main question would then be: Does the Providone prevent the synthises dH2o -MurAcid-HydroPerox from yielding Iodine Crystals?
 #2 
Old 2003-06-12, 00:33
pikk pikk is offline
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Default Re: Providone-Iodine Solution 10% Is this OK for push/pull I2 crystals?

i would not waste my time if i were you 1% it takes to much to get anywhere . cant swim find 2% at least . as for storage try a pill bottle works good . as for the ratio's for prov. idione could not tell you wont waste swims time with it..
 #3 
Old 2003-06-12, 04:58
DaMethuzereth DaMethuzereth is offline
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Default Re: Providone-Iodine Solution 10% Is this OK for push/pull I2 crystals?

Pikk, before you posted your reply, smim tried the synthesis and it seemed to work ok however, I ended up with a tar-like glop which weighed about 3.5 grams. It was almost bone dry and tar-like. Maybe swim messed up during the cleaning process, not sure. Can you elaborate? From now on however, swib will probably stick to the tincture iodine at 2%. cant find the 7% and swib is looking for the horsey hoof iodine.
 #4 
Old 2003-06-12, 05:06
pikk pikk is offline
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Default Re: Providone-Iodine Solution 10% Is this OK for push/pull I2 crystals?

prov has a tendcey to gum things up or at least with pills so it might do the same with i2 did you clean it real well with water . you could always sublime it but this is a pain in the ass .dont know i will look for some thing on this
 
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