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Laboratory Tips Safety proceedures, test reagents, drilling rubber stoppers, bending glass tubes, etc. Contributed to by chemists.

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 #1 
Old 2003-06-09, 01:18
stillbill stillbill is offline
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Default Timing the rxn?

After reading an answer to a question posted by a mistress, I would ask the question concerning curbshot's 2 can synth. about setting the timer for 1 hr. Now I'm reading

about 30 hr. nanos. for better product! Could someone explain?
 #2 
Old 2003-06-09, 01:51
Masahed Masahed is offline
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Default Re: Timing the rxn?

Well Swim feels kinda unqualified to answer given that some of the true pioneers are in our midst, but since CH is (temporarily, he hopes) down, he will attempt to answer.

Fuck the soupcans off, & the test-tube & go for a bottle (no more than 150ml), a salt shaker has been mentioned by a reliable source.

Pot of water is better than soupcans, temp always seems to differ from person to person but SwiM thinks 70-80c. Be sure to top up the water level if it gets low.

12hr MIN & up to 36 for kickass gear.

While SwiM beleives this to be true, he is stuck at the pfed extraction (sourcing problems) so he says he has not yet has the pleasure of verifying it.
 #3 
Old 2003-06-09, 01:55
acidmelt acidmelt is offline
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Default Re: Timing the rxn?

bro it all depends on so many factors. some are all about the reflux, others are about the traditional 1 to 2 hour cook. one of the factors that has a lot to do with it (besides personal opinion) is the cleanly-ness of your precursers. swia finds that it may be a better idea to go with the reflux if your precursers arent SUPER clean.
 #4 
Old 2003-06-09, 15:00
stillbill stillbill is offline
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Default Re: Timing the rxn?

Thanx you guys as always.
 
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